We will introduce a case study examining the optimal dispersion time using a bead mill through three measurement methods.
We would like to introduce a case study conducted by Majerika Japan Co., Ltd. that explored the dispersion endpoint of a concentrated slurry of barium titanate processed with a bead mill. Using a disperser, barium titanate was dispersed in a toluene-ethanol mixed solvent, and measurements were taken at various processing times to verify the results. From measurements using a rheometer, it was estimated that the over-dispersion boundary is 25.1 mm, and sedimentation velocity distribution measurements revealed that a significant amount of coarse particles were present after 33.4 minutes. 【Case Summary】 ■ Experiment - Relaxation time was measured using pulse NMR. - Viscosity and dynamic viscoelasticity were measured using a rheometer to determine the over-dispersion boundary and conditions for good dispersibility. - Sedimentation velocity distribution was determined using a centrifugal dispersion and particle size distribution measurement device. ■ Results - The over-dispersion boundary was estimated to be 25.1 mm. - It was found that a significant amount of coarse particles were present after 33.4 minutes. *For more details, please refer to the PDF document or feel free to contact us.
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Our company was established with the cooperation of Mageleka, Inc. in the United States and Resonance Systems in Germany. We engage in the import and sales of analytical instruments, as well as the sales of analytical consumables, contract measurement services, technical consulting, and collaborative research. We believe it is a great joy to assist, even in a small way, with research and quality control, and we will think together with you as closely as possible as analysts, so please feel free to contact us with your requests.