Determination of SADT using a small-scale reaction calorimeter (glass vial) in mL size.

A method for determining the thermal hazards of reactive chemicals using DSC measurement! Glass vials are the sample containers.

This document is a technical note explaining the determination of SADT (Self-Accelerating Decomposition Temperature) using a small-scale reaction calorimeter with a mL size (glass vial). We attempted SADT simulation using azobisisobutyronitrile (AIBN) to determine the thermal hazards of reactive chemicals through DSC measurements. In this note, we used a mL size small-scale reaction calorimeter, with a heating rate of 0.025 to 0.20 K/min, which is approximately 1/20 of the typical DSC measurement range of 0.5 to 8 K/min. We encourage you to read it. [Published Data (Excerpt)] - DSC data for 1 mg of AIBN (azobisisobutyronitrile) at 5 K/min - Heating rate of 0.025 K/min - Heating rate of 0.050 K/min - Heating rate of 0.20 K/min - Predictions of what kind of DSC measurement data can be obtained *For more details, please download the PDF or feel free to contact us.

Business Intelligence and Data Analysis