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Useful for contract analysis and contract testing! MSE testing equipment

You can analyze and measure the durability and strength of materials yourself! Automatic MSE testing! Automatically acquires characteristics and distributions in the depth direction from the material surface.

The device consists of a "physical etching (particle erosion) section" and an "erosion shape measurement section." By precisely eroding the sample surface and continuously acquiring depth measurements, it is possible to evaluate strength comparisons, strength cross-sectional distributions, thickness and strength of each layer, and in-plane strength distributions. This allows for the acquisition of a large amount of information in a short time on material surfaces that have been difficult to measure until now. It enables the quantification of subtle differences, such as comparing film strengths from different deposition processes or visualizing degradation levels at various depths, which can help determine the direction of development within the company. Additionally, the particle erosion method can be tested on objects that are not flat, including curved or complex shapes. Actual parts can be tested as they are.

  • Testing Equipment and Devices
  • Strength Testing Equipment
  • Other measurement, recording and measuring instruments

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Map of Solutions and Test Cases

What problems can be solved in the MSE exam? A list of actual examples.

Here are some excerpts of solutions that the MSE test can provide for material development. We are also happy to propose solutions that are not included in the MAP. Please feel free to consult with us.

  • Other measurement, recording and measuring instruments
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[Contract Analysis and Testing Examples] Introducing the Value of New Material Strength Testing through Manga

Achieving precise measurement of the strength of thin films, interfaces, and material surfaces. Innovations with new technology contribute to problem-solving and the advancement of products. You'll be convinced once you read it!

Palmeso has received various concerns regarding materials. - I want to know the strength of the thin film only. - I want to know the strength distribution of multilayer films and gradient films. - I want to know the changes in interfacial strength. - I want to know the degree and distribution of degradation. - I want information for optimizing the process. - There seem to be material properties that could not be understood with previous testing methods. When such issues arise, how do you solve the problems? Are you progressing with the project without confidence? This document explains the know-how gained from years of contract analysis and testing in a comic format! It tells the story of how MSE testing can contribute to solving material concerns that arise in development settings. Although MSE testing is contract analysis and testing, it is a completely new method, so we gently explain the technical points that may be difficult to understand in the comic. 【Features of MSE】 - It can measure the strength of the film alone without being affected by the substrate, even for ultra-thin films. - It can measure the strength distribution of each layer in multilayer films. - It can measure the strength distribution at the interface and before and after it. - It can measure the degree and distribution of degradation. - It can visualize effective process conditions. - It reveals the duality of materials, such as "hardness" and "brittleness."

  • Testing Equipment and Devices
  • Contract measurement
  • Other inspection equipment and devices

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[Test Case] Strength Evaluation of Steel Surface Treatment in the Depth Direction

We will introduce a case that visualizes how the hardness distribution varies significantly with each nitriding treatment.

We will introduce a case study that tested three types of nitriding treatments on the same material. As a result, it was found that there are weak areas on the surface, and that strength and thickness vary significantly depending on the treatment. 【Case Overview】 ■Objective - To identify the strength (hardness) distribution in the depth direction from the surface of shallow surface-treated materials. ■Evaluation - Gas nitriding achieved the minimum erosion rate (maximum hardness) at a depth of 8µm, remained constant up to 12µm, and then gradually increased the erosion rate (hardness decreased) until reaching 20µm, where it stabilized. *For more details, please refer to the PDF document or feel free to contact us.

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[Test Case] Ultra-precise film quality analysis of TiO2 optical thin films

Detailed explanation of the test results for multi-angular alumina particles/spherical silica particles.

We will introduce a case where optical films were tested using two types of particles: angular alumina particles and spherical silica particles, enabling an unprecedented level of ultra-precise analysis of film quality. The results from examining the angular alumina particles through an erosion rate (damage speed) distribution graph showed that "both the load at the time of impact and the contact area are extremely small, leading to concentrated force." 【Case Overview】 ■ Objective - To highlight slight differences in film quality using two types of testing conditions. ■ Test Results (Spherical Silica Particles) - Low hardness micro-spherical particles were used. - Although the load at the time of impact is large, the contact area is also large, resulting in dispersed force. *For more details, please refer to the PDF document or feel free to contact us.

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[Test Case] Degradation Diagnosis of Thermoplastic Resin Materials

Introduction to the relationship between nanoindentation and MSE testing.

We will introduce a case study on the evaluation of resin degradation characteristics in various environmental tests. As a result of examining the erosion rate distribution graph, we found that "the undegraded state has uniform strength throughout" and "thermal degradation occurs uniformly throughout," among other findings. 【Case Overview】 ■Objective - Evaluation of resin degradation characteristics in various environmental tests ■Evaluation - The rate of strength reduction is smaller compared to other types of degradation - PBT can be considered a material that is weak against moisture and heat, etc. *For more details, please refer to the PDF document or feel free to contact us.

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[Contract Analysis and Testing Examples] The strength of paint and coating films is measured precisely.

The method involves commissioned analysis and testing, allowing the durability of multi-layered coatings to be measured in the MSE test as "layer strength" and "interface strength"!

The technology for painting and coating has evolved tremendously, and there is an abundance of information about materials and processes. However, I have heard that those involved in development and adoption are struggling to make choices due to the overwhelming amount of information. This method involves contract analysis and testing, and while it could be done independently, the challenge lies in selecting the testing methods that will yield the desired information. When it comes to mechanical properties (strength), one piece of information we want to know is the continuous strength and distribution from the surface of a multilayer film to the substrate (fabric). Another aspect is the dual nature of hardness and brittleness, which reflects scratch resistance and impact resistance. **What can be done with MSE testing:** - It allows for precise measurement of continuous strength distribution from the surface to the substrate. → Regardless of the number of layers, the individual strength of each layer and interfacial strength can be understood, providing a clear cross-sectional profile of how each layer connects in terms of strength. - It can highlight the characteristics of hardness (Young's modulus) and toughness (brittleness). Please try the MSE test, which offers a new perspective that changes conventional testing concepts. We promise to provide information that will greatly assist in development and selection.

  • Testing Equipment and Devices
  • Contract measurement
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[Contract Analysis and Testing Examples] Life Design Starts with Accurate Measurement of Degradation Level

Manufacturing is greatly restricted by the sustainable international goals of the SDGs on Earth. We introduce MSE tests that are useful for material and process development.

The SDGs demand technological advancements aimed at reducing energy consumption, lightweighting, minimizing environmental impact, and extending lifespan in manufacturing. In materials, this translates to increased strength, enhanced functionality, and reduced manufacturing costs, necessitating boundary design and stable manufacturing technologies. This requires extensive trial and error and testing to accelerate development speed, making future IoT integration using AI essential. To create the necessary materials database (DB), it is crucial to have technology that accurately measures degradation lifespan based on material characteristics and aging. Future materials will involve not only material development but also multilayer and composite development. We have developed the MSE testing method as a means to quantify and compare the mechanical properties of a wide range of materials. **What can be done with MSE testing:** - Compare ceramics, metals, resins, and rubber materials on the same scale. - Visualize characteristics in hardness (Young's modulus) mode and toughness (brittleness) mode. - Obtain continuous distribution data from the surface to the interior of thin films and multilayer films. - Apply it to precisely test the degree of decline in mechanical properties due to material degradation. Please utilize this for high-speed screening of various material development processes and for creating a database of material strength.

  • Testing Equipment and Devices
  • Contract measurement
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Presentation of Case Study Materials! Verification of Differences in Automotive Painting Processes for the Automotive Industry

We are introducing a verification of the differences in automotive painting processes using case studies. This is a must-see for those struggling with durability analysis of paint films or painting processes!

We will present examples of performance comparisons due to differences in processes that reveal the functional characteristics of coatings. 【Process Details】 ● Sample 1 WET-ON-WET is a method where the curing process of the colored base layer is shortened, and after applying the clear layer, it is cured. ● Sample 2 A method where each layer is cured after application before the next layer is applied. 【Visualizing Strength Distribution with MSE Testing】 ■ Abrasion Resistance Distribution Test Condition 1: Cutting Mode ■ Toughness Characteristics Distribution Test Condition 2: Impact Mode 【Test Results】 It was found that the colored base layer and the clear layer in WET-ON-WET are smoothly connected. The above tests revealed that the WET-ON-WET process improves not only speed and energy efficiency but also painting quality based on the continuous strength distribution of the coating. Detailed results of the above tests can be viewed in the catalog. *For more information, please contact us or download the PDF materials for further details.

  • Impact Test
  • Automotive catalyst evaluation test equipment
  • Testing Equipment and Devices

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Case Study: "Characteristics of MSE Testing and Its Application to Organic Coatings"

We will introduce the features of the MSE test and other testing methods.

The MSE testing method allows for the measurement of the strength of a film independent of the substrate, as well as the continuous measurement of strength distribution from the surface to the interior. In this case, we verified whether the MSE test can truly analyze the strength of the film. 1. Comparison of film strength with different substrates 2. Comparison of film strength with different thicknesses 【Differences from other testing methods】 Example: Pencil test ● Pencil hardness - The thicker the film, the harder it becomes. - The harder the substrate, the harder it becomes. → This evaluates the functionality including both the film and the substrate. ● MSE test Does not depend on film thickness or substrate. → This evaluates the film itself and the substrate itself. The "MSE test" can be used for various applications such as material evaluation, investigation of strength distribution within the film, and defect analysis. *For more details, please contact us or download the PDF document to view.

  • Strength Testing Equipment
  • Automotive catalyst evaluation test equipment

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Case study: "How the strength changes with the material mixing ratio of organic coatings."

How does the strength change according to the prescription?

In the catalog, we present a relationship diagram that plots the results of two types of MSE tests: the horizontal axis represents "the strength of the material itself at the microscale," and the vertical axis represents "toughness at the macroscale: fatigue characteristics," from which we calculated MSE resistance (g/μm). [Various Changes] ● Changes due to differences in the materials used ● Changes due to the ratio of hardener components ● Changes due to the amount of photopolymerization initiator added *For more details, please contact us or download the PDF document to view it.

  • Coating Agent
  • Testing Equipment and Devices

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Case Study: Analysis of Film Quality and Durability Evaluation of Ultra-Hard Chip Surface Coating

Tests were conducted on two types of carbide tips for cast iron machining.

We would like to introduce a case study on the "Film Quality Analysis and Durability Evaluation of Coated Carbide Inserts." 【Objective】 ● Identify the multilayer structure of the film and conduct a comparative evaluation against design values. ● Evaluate the film strength that contributes to durability. 【Test Content】 For two types of carbide inserts used in cast iron machining, MSE tests were conducted to obtain the full layer distribution through a two-particle test for comparative evaluation. 【Test Results】 * For more details, please contact us; detailed test results can be viewed in distribution graphs. 【Customer Feedback】 ● Testing was possible while maintaining the chip shape, allowing for structural comparison with design values and precise strength inspection from the detailed strength distribution. ● Differences in "micro strength and homogeneity of the film" were highlighted from Test 1, and differences in "toughness of the film" were revealed from Test 2. ● Insights consistent with cutting durability were obtained from Test 2. * For more details, please contact us or download the PDF materials for further information.

  • Strength Testing Equipment
  • Coating thickness gauge

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[Matter] MSE Map

The direction of material development can be quickly confirmed! MSE map showing the duality of materials.

The MSE map is a method developed to visualize and quantify the conflicting duality inherent in materials, such as "hard and brittle." It has been made possible by obtaining erosion strength (erosion resistance rate) under different MSE testing conditions. We provide MSE maps for inorganic and organic materials. [Contents] ■ MSE maps for inorganic materials ■ MSE maps for organic materials ■ Utilization of MSE maps *For more details, please refer to the PDF document or feel free to contact us.

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[Test Case] Characteristics of Hard Thin Films and Substrates Observed in Two-Particle Tests

Detailed explanation of the test results for multi-angular alumina particles/spherical alumina particles.

We present a case study evaluating the properties of films and substrates from two tests under different conditions. The results observed from the erosion progression graph (damage progression) of spherical alumina particles indicated that "TiCN_1 is weaker than TiCN_2, and DLC_1 is stronger than DLC_2." 【Case Overview】 ■Objective - To evaluate the properties of films and substrates from two tests under different conditions. ■Test Results (Angular Alumina Particles) - The strength of the coating is stronger for DLC than for TiCN. - The strength distribution of the coating is a curve distribution for TiCN. - There is a weak layer present between the DLC and the substrate. *For more details, please refer to the PDF document or feel free to contact us.

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[Test Case] Comparison of Strength of Rubber Materials and Investigation of Surface Alteration Layer

A detailed explanation of the test results obtained for the strength distribution from the surface to the interior of various rubber sheets.

We will introduce a case study on the comparison of the strength of rubber materials and the investigation of the surface degradation layer. As a result of identifying the overall average erosion rate and the thickness of the surface degradation layer, we obtained test results such as "the inherent strength of the material becomes clear" and "the distribution from the surface to the interior can be visualized." 【Case Overview】 ■ Purpose - Comparison of the erosion strength of rubber materials - Investigation of the degradation layer that occurs on the surface of molded products ■ Evaluation - The inherent strength of the material becomes clear - The distribution from the surface to the interior can be visualized - The thickness and strength of the weak layer at the very surface become clear *For more details, please refer to the PDF document or feel free to contact us.

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