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Testing, Analysis and Measurement
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ミツバ環境ソリューション

addressGunma/Kiryu-shi/598, Shinrimachi
phone0277-74-5958
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last updated:Dec 22, 2022
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ミツバ環境ソリューション List of Products and Services

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Material and Defect Analysis: Physical Property Investigation

Investigation using microhardness tester (DUH), dynamic mechanical analysis (DMA), and viscoelastic measurements (rotational rheometer), etc.!

At Mitsuba Environmental Solutions, we conduct "physical property investigations." We primarily perform tensile tests, bending tests, and compression tests on resin materials, as well as hardness measurements, microhardness testing, and viscoelasticity tests. For example, in Differential Scanning Calorimetry (DSC), we can evaluate the thermal properties of materials (such as endothermic and exothermic reactions due to melting and crystallization, glass transition, specific heat capacity, and thermal history) based on changes in heat flow when the temperature is varied. 【Targets】 ■ Tensile tests, bending tests, compression tests (mainly on resin materials) ■ Hardness measurements (Rockwell hardness, Vickers hardness), microhardness testing (DUH) ■ Viscoelasticity tests (DMA, rheometer) ■ Thermal properties: DSC, TGA, TMA *For more details, please refer to the related links or feel free to contact us.

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Material and Defect Analysis: Investigation Case Studies

Examples of investigations related to foreign substances and contaminants, as well as analyses of material composition and generated substances will be introduced!

We would like to introduce a case study on "Material and Defect Analysis" that our company conducted. In the investigation of foreign substances and contaminants, we carried out material analysis of contaminants on mobile phone antenna plating and conducted research on rubber blooming, among other things. Additionally, we have numerous case studies related to product and component damage, as well as rust and corrosion. 【Case Studies】 ■ Investigation of foreign substances and contaminants ■ Investigation of product and component damage ■ Analysis of material composition and generated substances ■ Surface investigation of electronic components, contacts, and appearance products ■ Investigation related to material properties and product reliability testing ■ Investigation related to rust and corrosion *For more details, please refer to the related links or feel free to contact us.

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Material and Defect Analysis: Cleanliness Investigation

Detailed analysis of collected particles, including elemental analysis of metal contaminants, is possible! The particle size distribution can also be determined!

Mitsuba Environmental Solutions conducts "cleanliness investigations" of products. Foreign substances within the process are collected on a filter, and measurements of suspended particles and compositional analysis are performed. Analysis using MICRO QUICK (particle scanner for component cleanliness inspection) can analyze particle size, quantity, shape, and classification on the filter, and it is also possible to collect foreign substances for detailed analysis such as EDX and FT-IR. 【Features】 ■ Measurement of suspended particles and compositional analysis ■ Cleaning of products and collection of foreign substances on a filter (in accordance with VDA-19.1) ■ Analysis using MICRO QUICK ・ Capable of analyzing particle size, quantity, shape, and classification on the filter ・ Collection of foreign substances for detailed analysis such as EDX and FT-IR is also possible *For more details, please refer to the related links or feel free to contact us.

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Material and Defect Analysis: Confocal Microscope

A measuring microscope with high resolution! It is used for surface roughness measurement and shape measurement/comparison.

At Mitsuba Environmental Solutions, we conduct "confocal microscope measurements" using a confocal microscope. The laser microscope "OPTELICS HYBRID" manufactured by Lasertec can obtain high-resolution images with a sharp focus across the entire field of view on samples with uneven surfaces. It enables non-destructive, non-contact three-dimensional shape measurement. High magnification and high-resolution observation with a 405nm laser beam allows for clear visualization of ultra-fine structures. 【Measurement Range】 ■ Width Measurement - Minimum measurement unit: 0.001μm, measurement reproducibility: 3σ < 10nm ■ Height Measurement - Scale resolution: 0.4nm, measurement reproducibility: σ < 10nm, measurement range: 7mm *For more details, please refer to the related links or feel free to contact us.

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[Materials and Defect Analysis] X-ray Microfocus Inspection: X-ray CT Imaging

Pixel resolution is approximately 7 to 120 µm! Measuring voids in aluminum die-cast products and solder.

Our company conducts "X-ray Microfocus Inspection: X-ray CT Imaging." X-rays are irradiated onto the sample, which is rotated 360 degrees on the sample stage for imaging. This non-destructive method allows for the three-dimensional observation of a wide range of products, including the internal structure and defects of the sample. Due to the varying penetrability of X-rays, contrast is created based on the constituent elements (density). Elements with higher density appear bright, while those with lower density appear dark. 【Features】 - Target sample size: Diameter 150 × Height 170 mm (for vertical imaging) and up to 5 kg - X-rays are irradiated onto the sample, which is rotated 360 degrees on the sample stage for imaging - Enables three-dimensional observation of a wide range of products, including the internal structure and defects of the sample - Contrast is created based on the constituent elements (density) due to the varying penetrability of X-rays - Elements with higher density appear bright, while those with lower density appear dark *For more details, please refer to the related links or feel free to contact us.

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[Materials and Defect Analysis] Dynamic Ultra-Microhardness Tester

Evaluation of surface physical properties of a wide range of materials such as metals, plastics, rubber, and ceramics!

At Mitsuba Environmental Solutions, we conduct material and defect analysis using the "Dynamic Ultra-Micro Hardness Tester." The SHIMADZU "DUH-211S" measures the relationship between the load and indentation depth at micro areas of the surface (approximately 0 to 10µm) in real-time to evaluate surface properties. In a case comparing the surface hardness of enamel coatings on copper wires, it was found that "imported products have higher surface hardness and lower elastic modulus." 【DUH-211S Specifications】 ■ Test force: 0.1 to 1961mN, minimum measurement unit 0.196μN (for tests below 1.96mN) ■ Indentation depth measurement: 0 to 10μm, minimum measurement unit 0.0001μm ■ Indenter: Triangular pyramid indenter (angle between faces 115 degrees, Berkovich type) ■ Microscope magnification: 500x (objective 50x, eyepiece 10x) ■ Types of tests: 7 types *For more details, please refer to the related links or feel free to contact us.

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Material and Defect Analysis: Rotational Rheometer

The measurement temperature range is -130 to 500℃! It can measure thermal properties, mechanical properties, and rheological properties.

At Mitsuba Environmental Solutions, we conduct material and defect analysis using a "rotational rheometer." The "ARES-G2" manufactured by TA Instruments Japan Co., Ltd. can measure the thermal, mechanical, and rheological properties of polymer materials such as plastics and rubber. It employs a torsional excitation method, with measurement examples including frequency dependence, shear rate dependence, temperature dependence, and viscosity. 【ARES-G2 Specifications】 ■ Measurement temperature range: -130 to 500℃ ■ Torsional excitation method ■ Angular frequency range: 10^-7 to 628 rad/sec ■ Torque range: 0.05 μNm to 200 mNm ■ Strain range: 1 μrad to infinity ■ Geometry: Parallel plates (φ25, 50mm) *For more details, please refer to the related links or feel free to contact us.

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Material and Defect Analysis: Dynamic Mechanical Analysis (DMA)

It is possible to measure the elastic modulus and tanδ! By measuring stress or strain, the mechanical properties of the sample can be assessed.

Our company conducts dynamic mechanical analysis (DMA) of polymers. By applying a strain or stress that changes (vibrates) over time to the sample and measuring the resulting stress or strain, we assess the mechanical properties of the sample. When considered as a method of thermal analysis, it can be interpreted as a technique for measuring the mechanical properties of the sample as a function of temperature in response to vibrational loads (or strains). 【Features】 ■ Applicable to a wide range of materials by using different deformation modes ■ Capable of measuring temperature dependence and frequency dependence ■ Able to observe various relaxation phenomena, including glass transition ■ Provides information about the molecular structure and molecular motion of polymers *For more details, please refer to the related links or feel free to contact us.

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Material and Defect Analysis: Microplastic Analysis

There are three types of suspected samples! The collected particles are automatically counted in order of size, and the particles can be measured.

The issue of microplastic waste in oceans and rivers is gaining global attention. Our company conducts "microplastic analysis" (from sampling to particle measurement to particle material analysis) using pseudo-samples to address this issue. We added pseudo-samples to water, performed suction filtration, and dispersed them on filter paper to conduct particle counting measurements using light scattering analysis. 【Features】 ■ Three types of pseudo-samples ■ Added pseudo-samples to water for suction filtration and dispersion on filter paper ■ Conducted particle counting measurements using light scattering analysis ■ Automatically counted collected particles in descending order, allowing for particle measurement ■ Detailed analysis of counted particles is possible *For more information, please refer to the related links or feel free to contact us.

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