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  1. Home
  2. Testing, Analysis and Measurement
  3. 一般財団法人材料科学技術振興財団 MST
  4. [MST Homepage] Analysis Case "Heating Degradation Test of Lithium-Ion Secondary Batteries" Published
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  • Nov 21, 2011
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Nov 21, 2011

[MST Homepage] Analysis Case "Heating Degradation Test of Lithium-Ion Secondary Batteries" Published

一般財団法人材料科学技術振興財団 MST 一般財団法人材料科学技術振興財団 MST
The MST website has published analysis case studies. ◆Title Heating Degradation Test of Lithium-Ion Secondary Batteries ~Samples after heating degradation can be evaluated using LC/MS/MS, TOF-SIMS, TEM+EDX, etc.~ ◆Measurement and Processing Methods TOF-SIMS, TEM, LC/MS/MS, FIB, μ-sampling, lift-out, disassembly, atmosphere control ◆Product Field Secondary Batteries ◆Analysis Objectives Composition evaluation, identification, chemical bonding state evaluation, film thickness evaluation, degradation investigation, reliability evaluation ◆Overview The development of lithium-ion secondary batteries faces challenges such as performance enhancement, longevity, and reliability improvement. To address these challenges, understanding the degradation mechanisms of the batteries is crucial. In this instance, a heating degradation test was conducted to evaluate the degradation mechanisms due to temperature. After the heating degradation test, samples that showed significant capacity reduction were evaluated using LC/MS/MS for the electrolyte, TOF-SIMS for the anode surface, and FIB-TEM+EDX for the anode cross-section. ★★For detailed data, please refer to the link★★
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[Analysis Case] Heating Degradation Test of Lithium-ion Secondary Batteries
Samples after heating degradation can be evaluated using LC/MS/MS, TOF-SIMS, TEM+EDX, etc.
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[TOF-SIMS] Time-of-Flight Secondary Ion Mass Spectrometry

This is a method for structural analysis of the sample surface. Due to its sensitivity to the surface compared to other analytical devices, it is suitable for identifying organic contaminants on the very surface.

This is a method for structural analysis of sample surfaces. It is suitable for identifying organic contamination on the very surface due to its sensitivity compared to other analytical devices. Using a sputter ion source, it is possible to analyze the distribution of inorganic and organic materials in the depth direction. - Structural analysis and identification of organic and inorganic compounds are possible. - Coordination data from foreign substance inspection devices can be linked. - Qualitative analysis is possible from micron-order microforeign substances to several centimeters. - It is possible to analyze the very surface with high sensitivity. - Image analysis is possible. - Qualitative analysis of depth direction analysis is possible.

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(S)TEM (Scanning Transmission Electron Microscopy)

Elemental analysis, state evaluation, particle size analysis, and acquisition of three-dimensional structural images at the nanoscale.

TEM (Transmission Electron Microscopy) is a method that involves irradiating a thin sample with an electron beam, imaging the electrons that have passed through or scattered from the sample, and observing it at high magnification. ■ Advantages - Enlarged images can be obtained with sub-nanometer spatial resolution, allowing for the observation and analysis of the sample's fine structure and lattice defects. - It is possible to evaluate the crystallinity of the sample and identify materials. - By fabricating samples using FIB (Focused Ion Beam), it is possible to observe specific locations within a device with pinpoint accuracy. - By combining optional features, it is also possible to analyze the composition and state of localized areas. ■ Disadvantages - It is necessary to thin the sample (in some cases, thinning may be difficult for certain samples). - It does not observe individual atoms but rather displays average information in the thickness direction of the sample (typically about 0.1 μm thick). - Sample processing and observation may lead to alteration or deformation of the sample.

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一般財団法人材料科学技術振興財団 MST
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■■ Leak test for pouch containers such as packed rice! | MSQ-2003 series ■■ Packaging container air leak test device, pinhole inspection device, and full inspection device.

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The pinhole inspection for packaging engineering is fully automated, eliminating packaging defects based on certain quality standards. The judgment results and operational status can be managed via a monitor screen. - Quantitative management of quality standards for the pinhole inspection process - Ensuring the quality of the product's shelf life - Establishing evaluation criteria for the manufacturing process, achieving quantitative quality assurance - Slim and space-saving design that can be connected to existing production lines - Quick changeover for product variety switching can be handled in a short time by exchanging chambers - Fully domestically produced, allowing for rapid maintenance and troubleshooting - Example target works: pillow packaging, packaged rice (packaged cooked rice), etc. *Please consult us regarding the use of this product for pharmaceuticals.

Dec 08, 2025

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Notice Regarding Year-End and New Year Holidays

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We will be closed from December 27, 2025, to January 4, 2026. Inquiries during this period will be addressed sequentially after January 5. We apologize for the inconvenience and appreciate your understanding.

Dec 08, 2025

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Notice of Year-End and New Year Holidays

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Thank you very much for your continued support. We, at Marpos Co., Ltd., will be closed during the following period: Closure Period: From Saturday, December 27, 2025, to Sunday, January 4, 2026. Inquiries received during the closure period will be answered sequentially after the start of business in the new year. We apologize for any inconvenience this may cause and appreciate your understanding. Sincerely,

Dec 08, 2025

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Fukuda's leak test, leak inspection, leak detection, leak test, integrity test.

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Fukuda Co., Ltd. has been pursuing leak detection for 60 years and is committed to advancing the future of leak testing. 【 Supporting Various Leak Tests: Air Leak Test / Gas Leak Test (Hydrogen Gas, Helium Gas) 】 We develop, manufacture, and sell leak testing equipment to inspect airtightness and sealing properties. We will propose the appropriate testers and devices for each inspection target. 【 Target Industries and Examples of Inspection Targets 】 - Automotive Industry: Engines, FC components, valves and piping, various parts - Electronic Components Industry: Smartphones, keyless switches, various small sensors - Pharmaceuticals / Food / Cosmetics Industry: Bottle containers, syringes, vials, eye drop containers, pillow packaging, PTP packaging We will propose the most suitable leak testers for each industry. 【 ISO Certification 】JIS Q 9001:2015 (ISO 9001:2015)

Dec 08, 2025

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■■ Air Leak Tester | FLA-0200 / FLA-0201 series ■■ Fukuda's new flagship model. Equipped with mastering correction function, it enables high-precision measurements in a short time.

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Fukuda's new flagship model. - Masterless type (FLA-0200 series) - General type (FLA-0201 series) Two models of air leak testers. With the mastering correction function, high-precision measurements can be achieved in a short time. Please take a look at the catalog.

Dec 08, 2025

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