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  4. Evaluation of heat degradation rubber by DMA
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  • Jan 07, 2026
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Jan 07, 2026

Evaluation of heat degradation rubber by DMA

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This paper introduces the evaluation of thermally degraded rubber using dynamic viscoelastic measurements. A constant temperature chamber capable of circulating air within the chamber was used as a suitable device for thermal degradation testing, and NBR rubber and EPDM rubber were heated at 100°C for a specified time. The changes in viscoelastic behavior due to heating time were investigated. For both types of rubber, as the heating time increased, the tanδ (= E"/E') peak shifted towards higher temperatures, and a decrease in peak value was observed. It is believed that the loss of rubber elasticity and the decrease in elastic modulus resulted in the shift of Tg towards higher temperatures. By measuring dynamic viscoelasticity, it becomes possible to confirm the changes in physical properties associated with material degradation and to gain insights into structural changes. Additionally, conducting other chemical analyses can clarify more specific changes in chemical structure.
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thermal degradation_NBR rubber.png

Evaluation of thermal degradation rubber by DMA

Dynamic mechanical analysis (DMA) allows for the evaluation of the state from low to high temperatures.

This introduces the evaluation of thermally degraded rubber using dynamic viscoelasticity measurements. A constant temperature bath capable of circulating air within the chamber was used as a suitable device for thermal degradation testing, and NBR rubber and EPDM rubber were heated at 100°C for a specified duration. The changes in viscoelastic behavior due to heating time were investigated. For both types of rubber, as the heating time increased, tanδ (= E"/E') showed a peak that shifted towards higher temperatures, and a decrease in peak value was observed. It is believed that the loss of rubber elasticity and the decrease in elastic modulus resulted in a shift of Tg towards higher temperatures. By measuring dynamic viscoelasticity, it becomes possible to confirm the changes in physical properties associated with material degradation and to gain insights into structural changes. Additionally, conducting other chemical analyses can clarify more specific changes in chemical structure. [Test Overview] ■ A constant temperature bath capable of circulating air within the chamber was used ■ NBR rubber and EPDM rubber were heated at 100°C for a specified duration ■ Changes in viscoelastic behavior due to heating time were investigated *For more details, please download the PDF or feel free to contact us.

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Related catalog(7)

Evaluation of heat degradation rubber by DMA

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[Cast Iron Crack] We will repair cracks in metal products without applying heat.

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The "Mechanical Stitching Method" by Nichinichisui Road Machinery Co., Ltd. is a new technique that allows for the repair of metal cracks without the application of heat. By using special bolts and reinforcement plates, cracks are physically removed, and repairs are made without causing any thermal impact to the base material. Repairs can be carried out in environments where open flames cannot be used. Since no heat is applied, the disassembly of equipment is minimized. ◎ For more details, please contact us. ◎ If a detailed technical explanation is needed, please contact us.

Apr 15, 2026

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■■ Air Leak Tester | FLA-0200 / FLA-0201 series ■■ Fukuda's new flagship model. Equipped with mastering correction function, it enables high-precision measurements in a short time.

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Fukuda's new flagship model. - Masterless type (FLA-0200 series) - General type (FLA-0201 series) Two models of air leak testers. With the mastering correction function, high-precision measurements can be achieved in a short time. Please take a look at the catalog.

Apr 14, 2026

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[Cast Iron Crack Repair] We repair cracks in metal products without applying heat.

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The "Mechanical Stitching Method" by Nichinichisui Road Machinery Co., Ltd. is a new technique that allows for the repair of metal cracks without the application of heat. By using special bolts and reinforcement plates, cracks are physically removed, and repairs are made without causing any thermal impact to the base material. Repairs can be carried out in environments where open flames cannot be used. Since no heat is applied, the disassembly of equipment is minimized. ◎ For more details, please contact us. ◎ If a detailed technical explanation is needed, please contact us.

Apr 14, 2026

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[Free Catalog Distribution] Measures against "Near Misses" in Nursing and Care Settings. Prevent tripping and disconnection with codes! Wireless Series Bed Exit Sensors Linked to Nurse Call Systems.

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In facilities operating nurse call systems, we have made the bed exit sensor wireless, allowing it to notify in conjunction with the nurse call system. By simply connecting the mat sensor "Foldable Thin Matt-kun," the body movement call "Ugo-kun," and the wheelchair body movement call "Ayumi-chan" to the transmitter HB-RS, you can make the bed exit sensor wireless. The infrared sensor "Just Place Pole-kun" has the transmitter HB-RS built-in. This helps prevent accidents caused by falls, slips, or wandering, contributing to the efficiency of medical operations. 【Features】 ○ Wireless conversion by simply connecting existing sensors to the transmitter HB-WSK. ○ The bed exit sensor notifies wirelessly in conjunction with the nurse call system. ○ Up to 5 transmitters can be registered with a single receiver. ○ The communication distance between the transmitter and receiver is approximately 10 meters. ◎ For more details, please contact us or download the catalog.

Apr 13, 2026

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Non-contact light beam touch sensor "HA-T Series"

【Catalog now available!】Energy-saving automatic door sensors "HA-T401/HA-T520"

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The "HA-T Series" is an energy-saving automatic door sensor that opens only for those who wish to enter, whether on a busy street or in a narrow passageway. The automatic door opens simply by bringing your hand close, addressing hygiene concerns even in facilities used by a large number of people. You can choose between "Non-vision Mount Type/HA-T401" and "Non-vision Built-in Type/HA-T520" depending on the application and installation location. 【Recommended for such places!】 ☑ Entrance facing a busy corridor ☑ Presence of counters or signs near the door ☑ Buildings facing narrow passages ☑ Buildings that prioritize aesthetics ☑ Hospitals and facilities that consider hygiene ☑ Large facilities with many doors 【Features】 ● Adaptable to various door types with four detection spot settings ● Reduces unnecessary opening and closing, contributing to energy-saving by minimizing wasteful power consumption ● Equipped with a light touch function, allowing the door to open and close just by waving your hand, ensuring hygiene ● Can also be used as a wide detection range non-vision infrared sensor ◎ For more details, please download the materials or contact us.

Apr 13, 2026

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