Evaluation of Batteries Using the Isothermal Calorimeter TAM: Analysis Case Study
Isothermal calorimeter TAM series
As an evaluation method for self-discharge, it is a very sensitive technique. It allows for various assessments regarding battery performance, stability, and compatibility of constituent materials.
The isothermal calorimetry device (TAM series) is an instrument that measures very small amounts of heat, known as a microcalorimeter. By combining a thermostat with high isothermal performance with a calorimeter (calorimeter) suited to the sample and measurement method, it is possible to measure minute heat generated or consumed during physical processes or chemical reactions with sensitivity exceeding microwatts. Here, we introduce application examples of battery evaluation using the isothermal calorimetry device TAM. Additionally, information on the new battery calorimeter Micro XL is also provided. *Please download the materials.
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basic information
【Features】 ■ Up to 4 calorimeters can be mounted in 4 calorimeter positions ■ Calorimeters can be utilized in various configurations such as size and sensitivity ■ Up to 8 independent accessories can be controlled ■ New voltage I/O module for independent probe/source interface 【Specifications】 [Thermostat] ■ Heat transfer medium: Oil ■ Number of calorimeters: 4 ■ Temperature range: 4 to 150 ℃ ■ Accuracy: < ± 0.1 ℃ ■ Long-term stability: < ± 100 μ ℃/24h ■ Scan speed: ≤ ± 2 ℃/h
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Applications/Examples of results
■Stability and Storage Life Monitoring heat generation due to self-discharge in an open circuit ■Battery Performance Differences in thermal performance during charge and discharge cycles ■Evaluation of Possible Charge Cycles Impact of discharge conditions such as current magnitude, allowable terminal voltage of the battery, and temperature ■Quality Control Confirmation that there are no defects such as internal short circuits ■Research and Development Evaluation components for new electrochemical devices ■Compatibility of Components Evaluation of individual battery parts
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TA Instruments Japan is a wholly-owned subsidiary of TA Instruments in Japan. We sell and provide maintenance support for thermal analysis, rheology, microcalorimeters, and mechanical analysis equipment, conduct demonstration measurements, and hold technical seminars, offering the latest information on materials and engaging in the development of measurement technologies for materials. 【Main Equipment Handled】 ☆ Thermal Analysis / Differential Scanning Calorimeter (DSC), Thermogravimetric Analyzer (TGA), Simultaneous Differential Thermal Analysis (SDT/TG-DTA), Vapor Adsorption/Desorption Analyzer (Q5000SA) ☆ Viscoelastic Measurement (Rheology) / Rotational Rheometer (DHR・ARES), Dynamic Mechanical Analyzer (RSA・DMA・EF3200), Rubber Testing Cure Meter (RPA) ☆ Microcalorimetry / Isothermal Titration Calorimeter (ITC), Microcalorimeter (NanoDSC), Isothermal Calorimeter (TAM) ☆ Thermal Property Measurement Equipment / Thermal Conductivity Meter (DTC・FOX), Thermal Diffusivity Meter (DLF, DXF), Thermal Expansion Meter (TMA, DIL), Optical Thermal Expansion Meter (ODP, HM) ☆ Fatigue Testing Machines / ElectroForce Series, BioDynamic Series