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  6. [Case Study on Cost Reduction in the Laboratory] Reuse of Purified HFIP

[Case Study on Cost Reduction in the Laboratory] Reuse of Purified HFIP

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last updated:Oct 26, 2022

テクノシグマ
テクノシグマ
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Easy operation allows for unattended use! You can easily enhance labor (work hours), safety, and precision!

HFIP (hexafluoroisopropanol) is one of the few solvents that can dissolve many crystalline polymers. HFIP is an expensive solvent, with a price of around 100,000 yen per kilogram. While it is likely possible to purify and reuse HFIP by setting up a glass distillation apparatus yourself, many research and development environments face challenges in doing so. By introducing "Solpure," it is possible to significantly enhance the convenience, safety, and precision of HFIP distillation and purification. **Issues during HFIP distillation and purification:** - Due to its weight, a sturdy fixation is necessary when setting up larger equipment. - Care must be taken with pipes, seals, and grease that come into contact with HFIP vapor. - Although its toxicity is low, it has a strong odor and corrosiveness, making handling difficult. - It easily absorbs water, so a process to remove water is usually required. - Quality checks after purification are necessary. - Distillation and purification of one gallon bottle takes about two days. - High costs are incurred even when disposing of waste. *For more details, please refer to the PDF document or feel free to contact us.*

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[Case Study on Cost Reduction in the Laboratory] Reuse of Purified HFIP

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  • Related Link - https://techno-sigma.co.jp/costdown3/

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**Benefits of Using Solpure** ■ Easy operation and can be left unattended - Gallon bottles can be directly set into Solpure, eliminating the need for transferring containers - Molecular sieves can be added to the gallon bottle in advance for moisture removal - It operates automatically, allowing you to leave it unattended until processing of one bottle is complete ■ High durability - Designed to incorporate the use of HFIP (structure, strength, material quality, etc.) - Risks are minimized to the extreme ■ Safety - Purification is performed at low temperatures below the boiling point - Internal processing of the device is batch-type, preventing the concentration and accumulation of distillation residues - Automatically stops after purification is complete ■ Cost reduction - In GPC applications, it can be reused with a yield of approximately 90% or more *For more details, please refer to the PDF document or feel free to contact us.*

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HFIP Automatic Purification Device Solpure PSOS-HFIP

HFIP Automatic Purification Device Solpure PSOS-HFIP

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テクノシグマ

テクノシグマ

Industrial Electrical Equipment

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Techno Sigma Co., Ltd. and Creative Chemical Research Institute Co., Ltd. (our research and development division) provide organic solvent recovery devices and purification systems that guarantee a high-quality working environment in response to thorough energy conservation, resource saving, and effort reduction, all with the motto of being environmentally friendly, contributing to the prosperity of a new era. The roles of the two companies are that Creative Chemical Research Institute handles research and development as well as manufacturing, while Techno Sigma manages sales and marketing. Although they are different companies, they work closely together in the same location. The main customers are research and development and manufacturing divisions of universities in Japan and around the world (engineering, science, pharmacy, etc.), national research institutions, national research and development corporations, and companies related to pharmaceuticals, chemical industry, inorganic materials, polymer synthesis, electronic devices, medical products, natural products, and environmental measurement.

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