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  3. 石川工場
  4. Dependence of Zeolite Particle Distribution on Grinding Time
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  • Jan 15, 2024
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Jan 15, 2024

Dependence of Zeolite Particle Distribution on Grinding Time

石川工場 石川工場
**Summary** To understand the performance of the Ishikawa-type mixing and grinding machine produced at the Ishikawa factory, zeolite was used as the standard material to clarify the relationship between grinding time and particle size distribution through experiments. First, experiments were conducted using the D18S (desktop machine) to examine the relationship between the particle size distribution of zeolite and grinding time. The grinding times were varied at 15 minutes, 30 minutes, 1 hour, 2 hours, and 4 hours, with 2g samples taken at each interval. These samples were then analyzed for particle size distribution using a laser diffraction particle size measurement device. **Conclusion** In the particle size distribution, the peak value (mode) was 0.4μm for grinding times up to 1 hour. After 2 hours of grinding, it was 0.1μm. The standard deviation, which represents the variation in particle size, decreased with longer grinding times. However, beyond 2 hours, it saturated and remained almost constant at 3μm. From this, it can be concluded that within the experimental range, the relationship between the particle size distribution of zeolite and grinding time using the D18S shows that longer grinding times result in smaller particle size (mode) and less variation (standard deviation), but after 2 hours, it becomes constant.
Dependence of Zeolite Particle Distribution on Grinding Time
Dependence of Zeolite Particle Distribution on Grinding Time
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レーザ回折粒子径測定機を用いたD18Sにおけるゼオライト粒度分布の擂潰時間依存性について.pdf[607515]

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Product Information Details for D18S
This is the product information detail page for D18S, which was used to obtain data on the dependence of zeolite particle distribution on grinding time. D18S is a tabletop model equipped with two pestles, fully equipped with the performance of the Ishikawa-type stirring and grinding machine. Its stainless steel casing makes it suitable for physical and chemical experiments. Due to its unique technology, the trajectory of the pestles in the bowl is epicyclic, and the processing energy is lower compared to ball mills, making it suitable for mechanical alloying, mechanochemical, and mechanofusion processing.

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[Automatic Mortar] Ultra-compact, tabletop type, ideal for research and development environments Tiny

Optimal for pre-dispersion! Can mix and grind materials from just a few grams. Reproduces hand grinding【Compact Automatic Mortar】. Fits in a glove box at the smallest size!

【Features】 - The basic performance of the Ishikawa-type stirring and grinding machine is maintained while achieving a minimal size. - Processing volume is 0.03 liters. - An automatic mortar and pestle ideal for researchers and developers who perform grinding tasks manually with a mortar. - The pestle has a built-in spring, allowing for stirring and grinding while applying pressure. - Equipped with LED lighting for easy monitoring of processing conditions. - The detachable AC cord design makes it easy to move and store anywhere. - The use of a stainless steel casing improves chemical resistance, expanding its applications in laboratories and clean rooms. - Comes standard with an acrylic cover designed to prevent splashing and ensure safe handling. - Its ultra-compact and tabletop design allows for use within draft chambers or glove boxes, making it possible to grind substances containing organic solvents by selecting appropriate cover materials. 【Suitable Use Cases】 - Ideal as an automatic mortar and pestle in laboratories for various standard tests. - Dispersing, kneading, and grinding slurries, pastes, and colloids in an argon gas atmosphere using a glove box. - Achieving uniform dispersion and kneading during the concentration process of slurries and pastes with added solvents in a draft chamber through the stirring effect of the pestle and the grinding action of the pestle tip.

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Tabletop type, ideal for research and development environments: D101S/D16S Automatic Mortar and Pestle

Automation of porcelain mortar (mortar) and porcelain pestle (pestle). Ideal for a wide range of applications in food, pharmaceuticals, chemicals, and electronic materials, including stirring, grinding, kneading, and mixing.

The Ishikawa-type mixing and grinding machine is a device that can simultaneously perform "mixing," "grinding," "blending," and "kneading." With its unique structure, it achieves high-density particle uniformity and mixing uniformity. By adopting the same mortar and pestle used in manual work and automating the process, it contributes to improving product quality beyond manual methods, while also achieving reductions in work time and labor-saving efficiencies.

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Tabletop type, ideal for research and development environments: D20SL (manual lift type) automatic mortar and pestle.

The pestle rotation part rises and falls, making it easier to exchange the mortar and pestle, remove the ground material after grinding, and clean the machine. A tabletop machine for simultaneous stirring and dispersion processing.

**Features** - Achieves a compact design while retaining the characteristics of the Ishikawa-type stirring and grinding machine. - Improved chemical resistance due to the use of a stainless steel casing, expanding its applications in laboratories and clean rooms. - The elevation of the pestle rotation part makes it easy to replace mortars and pestles, retrieve ground materials after grinding, and clean the machine. - Being a tabletop model allows for use within draft chambers or glove boxes, enabling grinding of organic solvents and more. **Suitable Use Cases** - Ideal as an automatic mortar and pestle in laboratories for various standard tests. - Dispersing, kneading, and grinding slurries, pastes, and colloids in an argon gas atmosphere using a glove box. - Achieves uniform dispersion and kneading treatment during the concentration process of slurries and pastes with solvents added in a draft chamber, utilizing the stirring effect of the pestle and the grinding action of the pestle tip. - Compared to ball mills and planetary ball mills, it requires less processing energy, making it suitable for material development in mechanical alloying and mechanochemistry.

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  • Fine grinding machine

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"Compact, desktop type, ideal for research and development environments" D18S/D20S/D22S

Automation of mortar and pestle. Proven results in stirring, grinding, dispersing, kneading, and mixing for all-solid batteries, fine ceramics, carbon nanotubes, and conductive pastes.

【Features】 - Achieves a compact design while retaining the characteristics of the Ishikawa-type stirring and grinding machine. - Improved chemical resistance due to the use of a stainless steel casing, expanding its applications in laboratories and clean rooms. - The D18S, D20S, and D22S models feature two pestle tips, enhancing grinding performance. - Being a tabletop model allows for use within draft chambers and glove boxes, enabling grinding of organic solvents and more. 【Suitable Use Cases】 - Ideal as an automatic mortar in laboratories for various standard tests. - Dispersing, kneading, and grinding slurries, pastes, and colloids in an argon gas atmosphere using a glove box. - Achieves uniform dispersion and kneading treatment during the concentration process of slurries and pastes with added solvents in a draft chamber, utilizing the stirring effect of the pestle and the grinding action of the pestle tips. The Ishikawa-type stirring and grinding machine (Kakuhan Raikai machine) can simultaneously perform "stirring," "dispersion," "grinding," "mixing," and "kneading." This allows for processing effects that cannot be achieved with dedicated machines such as stirrers, dispersers, kneaders, and grinders, like in mechanochemical and mechanical alloying. Its unique structure realizes high-density particle shape uniformity and mixing uniformity.

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