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[Analysis Case] Surface Imaging of Soft Contact Lenses in Liquid AFM

Quantitative evaluation of surface properties can be performed using AFM analysis in an aqueous solution.

There are materials in polymers that change shape depending on the environment. To observe the original shape of the sample, measurements in real environmental conditions are necessary. This document presents a case study that visualizes the surface shape of soft contact lenses in saline solution. By measuring under conditions close to the actual environment, it is possible to evaluate while maintaining the original shape of the sample.

Company：一般財団法人材料科学技術振興財団　MST
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[Analysis Case] Evaluation of the Distribution of Drug Components Administered to the Eye

It is possible to process the eyeball and visualize the drug components (imaging).

Knowing how administered drugs distribute within the body is important information for drug development. In this case, the drug was directly administered into the vitreous body of fish eyes, and the distribution of the drug components was evaluated in cross-sections of the eyeball. As a result, the drug components were strongly detected near the administration site, showing their distribution within the eye. By using a mass microscope called TOF-SIMS, it is possible to apply this to the pharmacokinetics of various biological organs, including the eyeball.

Company：一般財団法人材料科学技術振興財団　MST
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[Analysis Case] Damage Assessment of Single Crystal Si Surface

Quantitative analysis of c-Si and a-Si by state is possible using high-resolution measurement and waveform analysis.

In the semiconductor manufacturing process, ion irradiation is sometimes performed for the purpose of surface modification. It is known that irradiating the surface of single-crystal Si with ions of inert elements can cause structural damage and lead to the formation of an amorphous layer. Utilizing the fact that high-resolution XPS spectra detect c (single-crystal) Si and a (amorphous) Si with different peak shapes, we will introduce a case where this damage-derived a-Si was separated from c-Si and quantitatively evaluated.

Company：一般財団法人材料科学技術振興財団　MST
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[Analysis Case] High Sensitivity Evaluation of SNDM's SiCMOS

The diffusion layer structure of SiC devices can be visualized (high-sensitivity evaluation of the diffusion layer structure).

In SNDM (Scanning Nonlinear Dielectric Microscopy), it is possible to identify the p/n polarity of semiconductors and visualize the shape of the diffusion layer. This method encompasses the functions of the traditionally used SCM (Scanning Capacitance Microscopy), allowing for sufficient evaluation of next-generation power devices, such as SiC, which are difficult to assess with SCM, from low to high concentrations. It is characterized by high sensitivity and can be applied to all compound semiconductor devices. As an example, we will introduce a case where a cross-section of a SiC Planer Power MOS was fabricated and analyzed using SNDM.

Company：一般財団法人材料科学技術振興財団　MST
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Contract Analysis
Transistor
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[SXES] Soft X-ray Emission Spectroscopy

SXES is a method that evaluates the chemical bonding state using soft X-rays emitted from materials.

- It is possible to evaluate the chemical bonding states focusing on specific elements in the sample (especially light elements such as B, C, N, O). - The spectral shape reflects the partial density of states of the targeted elements in the valence band. - Evaluation of the band structure is also possible through simultaneous measurement with X-ray absorption spectroscopy (XAS). - Since information from the bulk is obtained, it is less affected by the influence of the surface region within a few nanometers. - Evaluation can be performed without being affected by charging effects, even for insulators. - The detection limit is low (<1 atomic%), allowing for the evaluation of trace components.

Company：一般財団法人材料科学技術振興財団　MST
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[Analysis Case] Measurement of Organic and Inorganic Carbon Content in Food

It is possible to evaluate the carbon content of organic and inorganic substances in solids.

The total organic carbon analyzer (TOC analyzer) can quantitatively separate and measure total carbon (TC: Total Carbon) and inorganic carbon (IC: Inorganic Carbon) in a sample. The sample can be measured in its solid state without being dissolved in a solution. This document presents examples of TOC, TC, and IC evaluations in commercially available expanders and salts.

Company：一般財団法人材料科学技術振興財団　MST
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Evaluation of organic substances at the metal interface causing delamination.

TOF-SIMS can evaluate organic substances at metal interfaces in the depth direction.

Organic substances at metal interfaces can cause poor adhesion and delamination. For analyzing this poor adhesion, physically peeling off the layers and conducting qualitative analysis on the peeled surfaces is effective (refer to analysis case C0198). On the other hand, there are many cases where peeling cannot be performed, and in such cases, using a sputtering ion source for depth analysis is effective. This document presents a case of qualitative analysis of organic substances at metal interfaces, either in thin films or as secondary contamination, in the depth direction. As a conclusion, the presence of organic substances was confirmed by detecting C-series ions. Additionally, it is sometimes possible to identify organic substances by comparing them with known standard samples.

Company：一般財団法人材料科学技術振興財団　MST
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Ingredient analysis
Other analysis and evaluation services
analysis

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[Analysis Case] Depth Profile Concentration Analysis of Mg in Deep Ultraviolet LEDs

Quantification of impurities in AlGaN with various Al compositions is possible.

To determine impurity concentrations using SIMS analysis, it is necessary to use a standard sample with the same composition as the analysis sample. By preparing various Al compositions of AlGaN standard samples for AlGaN used in ultraviolet LEDs and power devices, MST can achieve more accurate quantification of impurities. We will introduce a case where, after disassembling a commercially available deep ultraviolet LED, SIMS analysis was conducted to determine the concentration of the dopant Mg and the distribution of the main component Al composition. Measurement method: SIMS Product fields: Lighting, power devices, optical devices Analysis purposes: Trace concentration evaluation, impurity evaluation, distribution evaluation, product investigation For more details, please download the materials or contact us.

Company：一般財団法人材料科学技術振興財団　MST
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Solid Analysis New Service Launch (GDMS)

We respond to your request to measure many elements with high sensitivity! Simultaneous analysis of over 70 elements, from major components to trace elements, is possible.

We have launched a new service using Glow Discharge Mass Spectrometry (GDMS) starting from May 15 (Monday). - Simultaneous analysis of over 70 elements, from major components to trace components at the ppb level, is possible. - Detection of C, N, and O at the ppm level, which was previously difficult. - Depth direction analysis is possible from nm to several tens of µm.

Company：一般財団法人材料科学技術振興財団　MST
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Contract measurement
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Combustion Ion Chromatography Analysis (Combustion-IC)

Analysis of halogens (F, Cl, Br) and sulfur is possible.

The combustion ion chromatography (IC) method allows for the investigation of the content of halogens (F, Cl, Br) and sulfur contained in solid materials such as plastics and resins, as well as in liquid materials like organic solvents. As shown in Figure 1, gases generated by combusting and decomposing the sample in a combustion furnace are collected in an absorbent solution. By measuring this absorbent solution using ion chromatography, it is possible to determine the content of halogens and sulfur in solid samples that are insoluble in water.

Company：一般財団法人材料科学技術振興財団　MST
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[Analysis Case] Measurement of Impurity Concentration on the Surface and Inside of SiC Substrates

Analysis of the substrate surface and interior is separated using ICP-MS and GDMS.

Impurities contained in semiconductor materials can affect product quality, leading to issues such as leakage current and early device failure. Therefore, understanding the amount of impurities in the materials is crucial for improving product quality. This document presents a case study on SiC substrates, which are gaining attention as power device materials, analyzing impurities adhered to the substrate surface using ICP-MS and impurities within the substrate using GDMS. Measurement methods: ICP-MS, GDMS Product fields: Power devices, manufacturing equipment, components Analysis purpose: Trace concentration evaluation For more details, please download the document or contact us.

Company：一般財団法人材料科学技術振興財団　MST
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Reproducibility of SIMS analysis data

It is possible to evaluate the amount of impurities with high reproducibility.

In the manufacturing of semiconductor devices, the control of impurities such as dopants is a crucial process. When focusing on ion implantation, even slight differences can affect quality and performance, making precise control necessary. The high reproducibility of SIMS analysis is ideal for the development and maintenance of these processes.

Company：一般財団法人材料科学技術振興財団　MST
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[Analysis Case] Organic Contamination Analysis of Materials

We will analyze trace amounts of organic contaminants adhered to the material using TD-GC/MS.

In precision machinery, vacuum devices, and semiconductor manufacturing equipment, contamination of the materials used can adversely affect product quality and the stable operation of the equipment. In this case, we handled glass components with disposable gloves of different types and analyzed the organic contamination adhered to the glass components using GC/MS analysis with a gas concentration device. By evaluating the contamination of the materials, it is possible to identify the components causing defects, eliminate the sources of material contamination, and consider changes to the materials.

Company：一般財団法人材料科学技術振興財団　MST
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Contract measurement
Semiconductor inspection/test equipment
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AFM Infrared Spectroscopic Analysis

Infrared spectroscopy is a method for obtaining information about molecular structure by measuring infrared absorption due to molecular vibrations.

This method allows for simultaneous measurement of the sample's surface roughness and mechanical property distribution, as well as infrared absorption images (functional group distribution) at selected absorption bands, by conducting measurements in conjunction with the AFM system. AFM-IR has the following features: - It enables evaluation with very high spatial resolution (on the nanoscale), allowing for spectral and imaging measurements in small areas. - Similar analyses can be performed by using the FT-IR library.

Company：一般財団法人材料科学技術振興財団　MST
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What can be understood from molecular dynamics calculations

We will introduce the target of analysis, the physical property information obtained, and examples of analysis that can be understood from molecular dynamics calculations.

In molecular dynamics simulations, the motion of particles (atoms and molecules) is simulated by applying Newton's equations of motion to individual particles, and the physical properties of the system are calculated based on statistical thermodynamics, along with evaluating the response and dynamics to external fields such as temperature and pressure. The results obtained are effective for predicting the structure and properties of materials and contribute to solving problems in research and development involving materials engineering and molecular biology.

Company：一般財団法人材料科学技術振興財団　MST
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[Analysis Case] Analysis of Functional Ingredient Concentration in Food

Evaluation case of resveratrol concentration in red wine.

Resveratrol is a type of polyphenol and a substance that has garnered attention as a natural antioxidant. Resveratrol, which is abundant in grape skins, is also present in red wine made from whole grape skins. This document presents an analytical case in which the amount of resveratrol in three types of commercially available red wine was measured and compared using the LC/MS/MS method.

Company：一般財団法人材料科学技術振興財団　MST
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[Analysis Case] Component Analysis of Food Wrap Film Surface

Analysis of the compositional changes on the surface of the wrap film before and after heating using TOF-SIMS.

We analyzed the surface components of three types of commercially available food wrap films (A, B, C) using TOF-SIMS. In this document, we focused on the outermost surface of the wrap films, as shown in Figure 1.

Company：一般財団法人材料科学技術振興財団　MST
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[Analysis Case] Composition and Impurity Analysis of Thin Films, Bulk, and Powder Materials

Quantitative analysis of main components and metallic impurity elements in IGZO using CP-MS.

IGZO thin films, which are transparent oxide semiconductors, are being researched and developed as TFT materials for displays. IGZO is a material whose properties change based on the composition of the thin film and the amount of impurities within it, making it important to obtain information about the composition and impurities. This time, we will introduce a case where the main components and the amounts of metallic impurity elements in IGZO powder, the raw material for the thin film, were evaluated with high precision using ICP-MS. Analysis is possible not only for powders but also for bulk and thin films.

Company：一般財団法人材料科学技術振興財団　MST
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[Analysis Case] Evaluation of Resistance Values and Li Distribution in Secondary Battery Cathodes

Distribution of resistance values in the electrode cross-section, visualization of conduction paths, and comparison with ion distribution.

The charge and discharge characteristics of lithium-ion secondary batteries are influenced by electronic conductivity. I will introduce a case where the decreased conductivity of active materials, due to degradation or blockage of conduction paths, was visualized as a resistance value distribution using SSRM. By comparing the results obtained from SSRM with the elemental distribution of Li and other elements measured by TOF-SIMS, it is possible to confirm the correlation between resistance values and elemental distribution. Additionally, it is feasible to classify conductive additives and binders based on resistance values, perform statistical processing, and quantify the mixing degree for each material.

Company：一般財団法人材料科学技術振興財団　MST
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[Analysis Case] Analysis of Bacteria Using DNA Analysis

We will analyze the bacteria in the sample from DNA without isolation or culture.

Bacteria have various growth environments depending on their species, and there are many bacteria that are difficult to isolate and culture. Therefore, by extracting and analyzing DNA, which is the blueprint of life that all bacteria possess, it becomes possible to investigate the existing bacteria without isolation or culture. Here, we will introduce examples of analysis methods for sequencing bacterial DNA to infer the existing bacteria through microbiome analysis, as well as investigating bacterial numbers using real-time PCR methods.

Company：一般財団法人材料科学技術振興財団　MST
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[Analysis Case] Mechanical Property Evaluation Simulation Using Molecular Dynamics Calculations

It is possible to analyze the deformation behavior of nanomaterials in response to environmental changes (pressure and temperature).

Carbon nanotubes (CNTs) are lightweight and possess excellent mechanical properties (high strength and high elasticity), making them suitable for various applications and environments. In particular, the deformation behavior of CNTs is related to flexibility and energy absorption characteristics, which are important in sensor and nano-device design. This document presents a case study that simulates the bending and recovery deformation of single-walled CNTs using molecular dynamics calculations. The simulation allows for the observation of structural changes at the atomic level due to environmental changes (pressure and temperature), enabling the analysis of deformation behavior based on the changes in strain energy associated with these structural changes.

Company：一般財団法人材料科学技術振興財団　MST
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[Analysis Case] Evaluation of Molecular Permeability to Lipid Bilayers through Molecular Dynamics Calculations

Insights into the permeability of molecules can be obtained from free energy calculations!

Our organization conducts evaluations of molecular permeability to lipid bilayers using molecular dynamics simulations. The free energy obtained from molecular dynamics calculations is an important value that contributes not only to predicting the stability of the system but also to understanding the material distribution and transport phenomena in systems with spatial and temporal fluctuations. For example, it is effective in gaining insights into the permeability of molecules across biological membranes. Using lipid bilayers in aqueous solvents as an example, we will introduce a case where the permeability of molecules in the membrane was discussed based on the free energy values when benzene and carbon dioxide were transported. [Measurement Methods and Processing Techniques] ■ Computational Science, AI, Data Analysis *For more details, please download the PDF or feel free to contact us.

Company：一般財団法人材料科学技術振興財団　MST
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Case Study Collection 2 on Thermal Analysis (DL Available/DSC)

We are thoroughly analyzing chocolate scientifically to explore differences in texture and melting behavior. We also have a proven track record in product comparisons, so please feel free to utilize our services.

In this case study collection, we will introduce examples related to "thermal analysis." Starting with "DSC Measurement of Chocolate 1 (Estimation of Crystal Type)," we also include "DSC Measurement of Chocolate 2 (Comparison Between Products)" and "DSC Measurement of Chocolate 3 (Differences in Melting Behavior)," along with their objectives, methods, and results. Additionally, we present analysis results, discussions, and other analytical examples. We encourage you to read it. [Contents] ■ DSC Measurement of Chocolate 1 (Estimation of Crystal Type) ■ DSC Measurement of Chocolate 2 (Comparison Between Products) ■ DSC Measurement of Chocolate 3 (Differences in Melting Behavior) ■ DSC Measurement of Chocolate 4 (Verification of Optimal Production Conditions) *For more details, please refer to the PDF document or feel free to contact us.

Company：セイコーフューチャークリエーション
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Analysis Services
Other polymer materials
analysis

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$Estimation of deformation and fracture due to compressive stress in plastic.$

Estimation of deformation and fracture due to compressive stress in plastic.

The deformation and fracture of plastic washers, gaskets, etc., due to localized compressive stress can be estimated using a TMA and stress-strain measurement device.

●Sample: Estimation of deformation and fracture due to localized compressive stress on plastic washers, gaskets, etc. ●Method: Compression creep measurement and stress-strain measurement using TMA (Thermomechanical Analysis) and stress-strain measurement equipment. ●Results: The deformation of the sample due to compression was understood from the creep curve and stress-strain curve. Please take a moment to read the PDF materials. In addition to TMA, our company also specializes in various thermal analyses such as DSC and TG/DTA. ●DSC: Can be used for analysis of sample melting, glass transition, thermal history, crystallization, curing, Curie point, etc., as well as measuring specific heat. ●TG/DTA: Can be used for analysis of moisture content, ash content, decomposition, oxidation, and evaluation of heat resistance. ●TMA: Can be used for measuring sample expansion rate, glass transition, softening point, etc. We would be happy to discuss this case and thermal analysis with you at any time. https://www.seiko-sfc.co.jp/service/thermal.html Case introduction https://www.seiko-sfc.co.jp/case/index.html *Other materials are also available. Please request them through the inquiry button, and we will send them to you.

Company：セイコーフューチャークリエーション
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Contract Analysis
plastic
Other polymer materials
analysis

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[DL Available/Thermal Analysis] DSC Measurement of Chocolate 1 (Estimation of Crystal Type)

DSC measurement allows for the understanding of the melting behavior of cocoa butter, the main component of chocolate. Please use it for texture discrimination and quality control of chocolate.

Differential Scanning Calorimetry (DSC) can be used for the analysis of sample melting, glass transition, thermal history, crystallization, curing, Curie point, and the measurement of specific heat. In this case, we introduce an analysis of chocolate, which is familiar to everyone, through "DSC Measurement of Chocolate 1 (Estimation of Crystal Type)." It is useful for distinguishing the texture (melt-in-mouth) of chocolate and for quality control, so please take a moment to read the PDF materials. In addition to DSC, our company also specializes in various thermal analyses such as TG/DTA and TMA. ● TG/DTA: Can be used for analyzing moisture content, ash content, decomposition, oxidation, and heat resistance evaluation. ● TMA: Can be used for measuring sample expansion rate, glass transition, and softening point. We also have a track record with other food products, so please feel free to consult us regarding thermal analysis. Case introduction https://www.seiko-sfc.co.jp/case/index.html *Other materials are also available. If you request through the inquiry button, we will send them to you.

Company：セイコーフューチャークリエーション
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Contract Analysis
Fats and oils
Organic Natural Materials
analysis

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[DL Available/Thermal Analysis] DSC Measurement of Chocolate 2 (Comparison Between Products)

By thoroughly scientifically analyzing chocolate, we can compare products from various companies.

Differential Scanning Calorimetry (DSC) can be used for analyzing the melting, glass transition, thermal history, crystallization, curing, Curie point, and measuring specific heat of samples. In this case, we introduce an analysis of familiar chocolate using DSC in "DSC Measurement of Chocolate 2 (Comparison Between Products)." This is the second installment. It is also useful for product comparison in determining the texture (melting) of chocolate, so please take a moment to read the PDF materials. In addition to DSC, our company specializes in various thermal analyses such as TG/DTA and TMA. ● TG/DTA: Can be used for analyzing moisture content, ash content, decomposition, oxidation, and evaluating heat resistance. ● TMA: Can be used for measuring expansion rate, glass transition, and softening point of samples. We also have experience with other food products, so please feel free to consult us regarding thermal analysis. Case Introduction https://www.seiko-sfc.co.jp/case/index.html *Other materials are also available. If you request through the inquiry button, we will send them to you.

Company：セイコーフューチャークリエーション
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Contract measurement
Food Testing/Analysis/Measuring Equipment
Organic Natural Materials
analysis

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Data DL available: FIB - Nano-level high-precision processing by FIB

The FIB device allows for high-precision processing at the desired position on a Si substrate without a mask at the nano level.

The FIB (Focused Ion Beam) system allows for maskless etching processing to create arbitrary shapes. In this case, we introduce the fabrication of pillars at 50nm steps with the following sizes: - Circular: φ5μm - Pillar height: 700nm/650nm/600nm - Pillar diameter: φ500nm Please take a moment to read the PDF materials. Additionally, our company specializes in wiring modifications aimed at circuit corrections for ICs and LSIs using FIB. Specifically, we offer the following services: - Cutting of wiring - Connecting of wiring - Fabrication of test pads for characteristic evaluation We perform these services with a short turnaround time to assist in your IC and LSI development. We would be happy to discuss this further, so please feel free to reach out. *If you need more details, please do not hesitate to contact us. Seiko Future Creation Official Website https://www.seiko-sfc.co.jp/

Company：セイコーフューチャークリエーション
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Processing Contract
Contract Analysis
Other semiconductors
analysis

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Introduction to Temperature Modulated DSC Method (Evaluation of Polymer Materials)

Temperature-modulated DSC allows for specific heat measurements using the IS method, providing a wealth of information in high-temperature regions where specific heat measurements have been considered difficult, which cannot be obtained with conventional DSC.

Temperature-modulated DSC provides a wealth of information that cannot be obtained with conventional DSC, enabling the following: - Distinction of thermal history, etc., through comparison of reversible and irreversible components as mentioned above. - Measurement of specific heat in high-temperature regions above around 1000°C, which is considered difficult with the JIS method. - Measurement of specific heat in low-temperature regions below room temperature. Additionally, it is expected to be useful for analyzing relaxation phenomena. In this case, as an example of that technology, we introduce "a case study evaluating PET." For more details, please refer to the PDF materials. Furthermore, in addition to DSC, our company also specializes in various thermal analyses such as TG-DTA and TMA. ● DSC (Differential Scanning Calorimetry): Can be used for analysis of sample melting, glass transition, thermal history, crystallization, curing, Curie point, etc., and for measuring specific heat. ● TG-DTA (Thermogravimetric and Differential Thermal Analysis): Can be used for analysis of sample moisture content, ash content, decomposition, oxidation, and heat resistance evaluation. ● TMA (Thermomechanical Analysis): Can be used for measuring sample expansion rate, glass transition, softening point, etc. For more information, visit here: https://www.seiko-sfc.co.jp/analysis-service/thermal-analysis.html

Company：セイコーフューチャークリエーション
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Other polymer materials
Contract Analysis
plastic
analysis

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Fixed-type X-ray inspection device for bags and parcels

Simple operation with just a push of a button.

Inspection device for bundles of letters, packages, and luggage.

Company：メルク
Price：Other

Other measurement, recording and measuring instruments
analysis

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Analysis of "Water Purifier Test"

Corresponding to various removal target substances! Water purifier testing by Hyogo Analysis Center Co., Ltd.

We conduct performance tests for household water purifiers, including "filtration flow rate tests," "removal performance tests," and "filtration capacity tests" as specified in the testing method "JIS S 3201," as well as performance tests for reverse osmosis (RO) water purifiers. Hyogo Analysis Center Co., Ltd. is recommended as a certified testing facility by the Japan Water Purifier Association. 【Features】 ■ Supports various target substances for removal ■ Recommended as a certified testing facility by the Japan Water Purifier Association For more details, please contact us or download the catalog.

Company：兵庫分析センター
Price：Other

Public Testing/Laboratory
analysis

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