ティー・エイ・インスツルメント・ジャパン List of Products and Services

The Discovery Core Rheometer is the first system to provide extensive measurements of viscosity and viscoelasticity with simple operability. New feature: The RheoGuide user interface allows operation from a touchscreen, providing guidance, visualization, and verification at each step. 【Discover Insights Beyond Viscosity】 Viscometers only report a single viscosity value within a limited range, while the Core Rheometer captures a complete viscosity profile, representing material behavior under all relevant conditions. Complex fluids such as suspensions, emulsions, gels, pastes, and slurries are non-Newtonian fluids, and their viscosity changes depending on the applied shear rate and time. Characterizing the full range of viscosity is crucial for understanding flow behavior under real-world conditions. Related link: https://www.tainstruments.com/viscometer-vs-rheometer-discover-why-a-rheometer-offers-more-than-just-viscosity-measurement/

• Analytical Equipment and Devices

The DCR (Discovery Core Rheometer) provides precision and detailed analysis that surpasses traditional viscometers in evaluating the flow characteristics of electrode slurries. The flow characteristics of electrode slurries are crucial factors that directly impact battery performance and lifespan. Conventional viscometers can only measure viscosity at a single shear rate, whereas the DCR analyzes flow characteristics in a wide range of shear rates, assessing the uniformity and stability of the slurry. This enables optimization of the manufacturing process and improvement of product quality. Key Features: - High-precision measurement: Accurately measures fine flow characteristics that cannot be detected by viscometers. - Wide shear rate range: Analyzes detailed flow characteristics to accommodate various manufacturing conditions. - Real-time analysis: Evaluates flow characteristics during the manufacturing process in real-time, providing immediate feedback. - Ease of use: Intuitive operation and advanced data analysis functions make it easy for anyone to use. By using the DCR, you can fully understand the flow characteristics of electrode slurries, enhancing battery performance and reliability. The DCR, which provides detailed data not obtainable from viscometers, is the optimal solution for battery manufacturing.

• Analytical Equipment and Devices

The DCR (Discovery Core Rheometer) provides precision and detailed analysis that surpasses traditional viscometers in evaluating the viscosity and viscoelasticity of hand creams and shampoos. The feel and performance of hand creams and shampoos heavily depend on their viscosity and viscoelastic properties. Conventional viscometers can only measure viscosity at a single shear rate, but the DCR analyzes viscosity and viscoelastic properties across a wide range of shear rates, allowing for the assessment of product feel and stability. This enables optimization in product development and quality control. Key Features: - High-precision measurement: Accurately measures fine viscoelastic properties that cannot be detected by viscometers. - Wide shear rate range: Adapts to various usage conditions and analyzes detailed viscoelastic properties. - Real-time analysis: Evaluates viscosity and viscoelastic properties in real-time during the manufacturing process. - User-friendly: Intuitive operation and advanced data analysis functions make it easy for anyone to use. By using the DCR, you can fully understand the viscosity and viscoelastic properties of hand creams and shampoos, enhancing product feel and quality. The DCR provides detailed data that cannot be obtained from traditional viscometers, making it the optimal solution for the development and quality control of personal care products.

• Analytical Equipment and Devices

The Discovery Core Rheometer is the first system to provide extensive measurements of viscosity and viscoelasticity with simple operability. New feature: The RheoGuide user interface allows operation from a touchscreen, providing guidance, visualization, and verification at each step. 【Discover Insights Beyond Viscosity】 Viscometers only report a single viscosity value within a limited range, whereas the Core Rheometer captures a complete viscosity profile, representing the material's behavior under all relevant conditions. Complex fluids such as suspensions, emulsions, gels, pastes, and slurries are non-Newtonian fluids, and their viscosity changes depending on the applied shear rate and time. Characterizing the full range of viscosity is crucial for understanding flow behavior under real-world conditions. 【Key Features】 Advantages of the Rheometer: ■ Accuracy and precision ■ Wide range of measurements ■ Controlled shear rate ■ Reproducibility of process conditions ■ Measurable with small sample sizes ■ Rapid temperature control Test Modes: ■ Flow ■ Oscillation ■ Transient

• Analytical Equipment and Devices

The TA Instruments RS-DSC (Rapid Screening Differential Scanning Calorimeter) is a device that brings innovation to the thermal stability testing of biopharmaceuticals. The RS-DSC enables laboratories to make more informed decisions and shorten time to market through high efficiency and streamlined analysis. Features of the RS-DSC: ■ Acceleration of thermal stability testing: Analyzes up to 24 samples simultaneously, providing detailed insights quickly. It also simplifies the characterization of high-concentration pharmaceuticals. ■ Improved efficiency: Utilizes disposable MFC (microfluidic chips) to operate efficiently with samples of less than 15μl. It eliminates the hassle of sample dilution and equipment cleaning, reducing contamination risks. ■ Informed decision-making: The NanoAnalyze software processes vast amounts of data, providing detailed and accurate insights into the thermal stability and thermodynamic properties of molecules.

• Analytical Equipment and Devices

Emulsions, suspensions, and other structurally viscous materials exhibit diverse flow curves and require complex interpretations. To complement this interpretation, we have developed a sensor that can simultaneously measure dielectric constant and impedance while controlling temperature in the flow field. - Simultaneous evaluation of steady flow viscosity (flow measurement), dynamic viscoelasticity, and electrochemical properties - Measurable over a wide AC frequency range (4 Hz to 8 MHz) - Easily attachable to a Peltier temperature control plate - Integrated control of rheo-impedance/rheo-dielectric measurements with TRIOS software

• Analytical Equipment and Devices

The "ODP 868," a result of over 20 years of research and development on optical testing devices for analyzing the thermomechanical behavior of materials, enables sample analysis that surpasses the limitations of conventional heating microscopes. With its multifunctionality, the ODP 868 is a highly innovative tool suitable for optimizing industrial processes related to manufacturing, research and development, and thermal cycles. The heating microscope mode uses a 5Mpix high-resolution camera to analyze the physical behavior of materials during industrial firing cycles. Through practical morphometrics, it calculates and visualizes various characteristic temperatures and parameters selected by the user in real-time during analysis. The ODP 868 can analyze samples of a wide range of shapes and sizes (for example, measuring 3mm and 10mm samples simultaneously) and can analyze up to 8 ISO standard-sized samples at the same time.

• Analytical Equipment and Devices

This is a material testing machine that uses linear motors manufactured by Bose Corporation, known for its audio equipment. It can conduct low-load tests more accurately across a wide range from low to high speeds. - The linear motor comes with a 10-year warranty and is maintenance-free. - Maximum frequency: 300Hz (for the 3200 series). - Ideal for low-load testing as there are no bearings or seals in the drive unit. - Usable in clean rooms. Here are the features of the ElectroForce 5500! - The smallest TA device. - In addition to tensile/compression/three-point bending, it can also perform viscoelastic/fatigue/immersion tests. - Fatigue testing can be conducted with loads that simulate human walking. - Up to 24 specimens can be measured simultaneously.

• Testing Equipment and Devices

Powder materials are used in various fields such as polymers, pharmaceuticals, and battery materials. In addition to general physical properties like particle size and density, these powders can take various forms such as storage, flow, and agglomeration, making it necessary to evaluate their physical properties while considering the environment in which they will be used. To effectively evaluate these physical properties with high precision and convenience, a new powder accessory for HR rheometers was launched in 2022. In this instance, we will focus on "graphite for batteries" and present a case study of powder rheology analysis.

• Analytical Equipment and Devices

Are you aware that TA's analytical instruments are playing a vital role in the manufacturing of "batteries," which are essential in modern life? TA's thermal analysis instruments, viscoelasticity measurement devices, thermal expansion measurement devices, and fatigue testing machines are equipped with a variety of measurement modes, enabling measurements across a wide range of fields. This time, we will focus on "batteries and electronic components" and present some analysis cases. 【Agenda】 P2~ Announcement of the Beyond 5G/6G Electronic Materials Seminar held in October 2021 You can also register from the link below! https://www.tainstruments.com/webinarlistjp/?lang=ja P3~ Introduction of DHR (rotational rheometer/viscoelasticity measurement device) Case study of viscoelasticity measurement of slurries P6~ Introduction of TAM (isothermal calorimeter) Battery product evaluation case 1 (heat measurement during open-circuit self-discharge) Battery product evaluation case 2 (effect of reducing side reactions of electrolyte additives)

• Analytical Equipment and Devices

Measurement capabilities offered by TA Instruments ☆ Thermal analysis / glass transition, crystallization, thermogravimetric analysis, curing reactions, expansion rate, thermal conductivity, shrinkage rate, effects of moisture, etc. ☆ Viscoelastic measurements (rheology, rheometers) / viscoelasticity, elastic modulus, viscosity, stress relaxation, creep, master curves, residual strain, molecular weight, molecular weight distribution, etc. ☆ Microcalorimetry / intermolecular interactions, crystallization, amorphousness, aggregation/precipitation, dispersibility, solubility, compatibility, wettability, stability, adsorption, etc. ☆ Fatigue testing / tensile strength, temperature dependence, viscoelasticity, elastic modulus, viscosity, stress relaxation, creep, master curves, residual strain, etc.

• Analytical Equipment and Devices

Measurement capabilities offered by TA Instruments ☆ Thermal analysis / glass transition, crystallization, thermogravimetric analysis, curing reactions, expansion rate, thermal conductivity, shrinkage rate, effects of moisture, etc. ☆ Viscoelastic measurements (rheology, rheometers) / viscoelasticity, elastic modulus, viscosity, stress relaxation, creep, master curves, residual strain, molecular weight, molecular weight distribution, etc. ☆ Microcalorimetry / intermolecular interactions, crystallization, amorphousness, aggregation/precipitation, dispersibility, solubility, compatibility, wettability, stability, adsorption, etc. ☆ Fatigue testing / tensile strength, temperature dependence, viscoelasticity, elastic modulus, viscosity, stress relaxation, creep, master curves, residual strain, etc.

• Analytical Equipment and Devices

The viscoelastic measurement device rheometer "Discovery Hybrid Rheometer" controls the surrounding environment and performs measurements over a wide range of force, strain, and strain rate. We offer three models to meet the needs for sensitivity and capability, ranging from the high-sensitivity HR-30 to the general-purpose HR-10. This product improves various performances and specifications, achieving accurate strain, strain rate, stress control, and normal force, and is equipped with our innovative patented Smart Swap geometry and Smart Swap temperature control system. 【Main Features】 ■ Ultra-low inertia drag cup motor (patented) ■ Magnetic bearings (patented) ■ High-resolution optical encoder ■ Optical encoder dual reader (patent pending) ■ Normal force rebalance transducer (FRT)

• Analytical Equipment and Devices

The "ARES-G2" is an advanced rotational viscoelastic measurement device/ rheometer for research and material development. It is equipped with dedicated actuators for deformation control for independent shear stress and normal stress measurements, as well as a torque balance transducer (TRT) and a force balance transducer (FRT). It allows for measurements free from device-induced effects across a wide range of stress, strain, and frequency. 【Features】 ■ Excellent data accuracy ■ Superior strain and new stress control ■ Fully integrated high-speed data sampling ■ Isolated power supply ■ New Smart Swap environmental system

• Analytical Equipment and Devices

The viscoelastic measurement device "Discovery Hybrid Rheometer" controls the surrounding environment and performs measurements over a wide range of force, strain, and strain rate. We offer three models to meet the needs for sensitivity and capability, ranging from the high-sensitivity HR-30 to the versatile HR-10. This product improves all performance and specifications, achieving accurate strain, strain rate, stress control, and normal force, and is equipped with our innovative patented Smart Swap geometry and Smart Swap temperature control system. 【Main Features】 ■ Ultra-low inertia drag cup motor (patented) ■ Next-generation magnetic bearings (patented) ■ High-resolution optical encoder ■ Optical encoder dual reader (patent pending) ■ Normal force rebalance transducer (FRT)

• Analytical Equipment and Devices

TA Instruments continues to be the leading company in the world of DSC with innovative and exceptional technology. It provides reliable data and enhances workflow and productivity in laboratories. Material property analysis is essential at all stages of product design, manufacturing, processing, and application. Differential Scanning Calorimetry (DSC) is the most widely used thermal analysis instrument for evaluating the physical properties of a wide range of materials, including polymers, pharmaceuticals, food, biomaterials, organic compounds, inorganic compounds, and composites.

• Analytical Equipment and Devices

This product adopts a patented "magnetic levitation balance" and allows for the evaluation of the vapor adsorption and desorption behavior of samples under various pressure conditions.

• Other weight measuring instruments

This document provides a detailed introduction to the characterization of pharmaceutical substances using Differential Scanning Calorimetry (DSC). It explains the "Modulated DSC," which allows for high-sensitivity and high-resolution measurements, and the "Tzero DSC," which measures the absolute values of heat flow, over more than 40 pages based on general characterization examples. You can also find an introduction to various analytical instruments offered by our company. 【Main Contents】 ■ Amorphous structure (detection of amorphous content in crystalline compounds including glass transition) ■ Degree of crystallinity (melting and crystallization, purity, polymorphism) ■ Drug-excipient interactions ■ Protein denaturation ■ Freeze-drying ■ Other complementary thermal analysis techniques *This document is available for immediate viewing via "PDF Download."

• Analytical Equipment and Devices

Measurement capabilities offered by TA Instruments ☆ Thermal analysis / glass transition, crystallization, thermogravimetric analysis, curing reactions, expansion rate, thermal conductivity, shrinkage rate, effects of moisture, etc. ☆ Viscoelastic measurements (rheology, rheometers) / viscoelasticity, elastic modulus, viscosity, stress relaxation, creep, master curves, residual strain, molecular weight, molecular weight distribution, etc. ☆ Microcalorimetry / intermolecular interactions, crystallization, amorphousness, aggregation/precipitation, dispersibility, solubility, compatibility, wettability, stability, adsorption, etc. ☆ Fatigue testing / tensile strength, temperature dependence, viscoelasticity, elastic modulus, viscosity, stress relaxation, creep, master curves, residual strain, etc.

• Analytical Equipment and Devices

Features and Benefits - Patented linear motor and high-resolution displacement sensor provide excellent data through control over a wide range of loads, displacements, and frequencies. - Extremely durable, frictionless motor with a 10-year warranty allows for maintenance-free and reliable operation. - High load capacity of 500N enables testing of larger samples or final products under actual conditions by achieving higher load levels in DMA and fatigue analysis. - Force Convection Oven (FCO) offers excellent control and responsiveness over a temperature range of -150 to 600°C. - Large Sample Oven (LSO) accommodating a temperature range of -150 to 315°C features spacious design for testing large samples or components. - Air Chiller System (ASC) utilizes unique gas flow cooling for low-temperature testing without liquid nitrogen, eliminating potential hazards in the lab while achieving remarkable return on investment. - Extremely robust test frame and air bearings ensure the highest precision results for high-rigidity samples.

• Testing Equipment and Devices

Measurement capabilities offered by TA Instruments ☆ Thermal analysis / glass transition, crystallization, thermogravimetric analysis, curing reactions, expansion rate, thermal conductivity, shrinkage rate, effects of moisture, etc. ☆ Viscoelastic measurements (rheology) / viscoelasticity, elastic modulus, viscosity, stress relaxation, creep, master curve, residual strain, molecular weight, molecular weight distribution, etc. ☆ Microcalorimetry / intermolecular interactions, crystallization, amorphousness, aggregation/precipitation, dispersibility, solubility, compatibility, wettability, stability, adsorption, etc. ☆ Fatigue testing / tensile strength, temperature dependence, viscoelasticity, elastic modulus, viscosity, stress relaxation, creep, master curve, residual strain, etc.

• Analytical Equipment and Devices

Measurement capabilities offered by TA Instruments ☆ Thermal analysis / glass transition, crystallization, thermogravimetric analysis, curing reactions, expansion rate, thermal conductivity, shrinkage rate, effects of moisture, etc. ☆ Viscoelastic measurement (rheology) / viscoelasticity, modulus of elasticity, viscosity, stress relaxation, creep, master curve, residual strain, molecular weight, molecular weight distribution, etc. ☆ Microcalorimetry / intermolecular interactions, crystallization, amorphousness, aggregation/precipitation, dispersibility, solubility, compatibility, wettability, stability, adsorption, etc. ☆ Fatigue testing / tensile strength, temperature dependence, viscoelasticity, modulus of elasticity, viscosity, stress relaxation, creep, master curve, residual strain, etc.

• Analytical Equipment and Devices

Measurement capabilities offered by TA Instruments ☆ Thermal analysis / Glass transition, crystallization, thermogravimetric analysis, curing reactions, expansion rate, thermal conductivity, shrinkage rate, effects of moisture, etc. ☆ Viscoelastic measurements (rheology) / Viscoelasticity, elastic modulus, viscosity, stress relaxation, creep, master curve, residual strain, molecular weight, molecular weight distribution, etc. ☆ Microcalorimetry / Intermolecular interactions, crystallization, amorphousness, aggregation/precipitation, dispersibility, solubility, compatibility, wettability, stability, adsorption, etc. ☆ Fatigue testing / Tensile strength, temperature dependence, viscoelasticity, elastic modulus, viscosity, stress relaxation, creep, master curve, residual strain, etc.

• Analytical Equipment and Devices

The planar biaxial testing machine (TestBench testing device) is designed to conduct tests similar to those performed on a load frame. This allows for the evaluation of the sample's stiffness, strength, and durability, as well as the measurement of yield strength, ultimate strength, and fatigue life. A modular approach that includes multi-channel and multi-axis options enables a wide range of configurations and performance. It uses 200N and 400N ElectroForce linear motors mounted on a horizontal base plate to accommodate various testing needs.

• Analytical Equipment and Devices

Measurement capabilities offered by TA Instruments ☆ Thermal analysis / glass transition, crystallization, thermogravimetric analysis, curing reactions, expansion rate, thermal conductivity, shrinkage rate, effects of moisture, etc. ☆ Viscoelastic measurements (rheology) / viscoelasticity, elastic modulus, viscosity, stress relaxation, creep, master curve, residual strain, molecular weight, molecular weight distribution, etc. ☆ Microcalorimetry / intermolecular interactions, crystallization, amorphousness, aggregation/precipitation, dispersibility, solubility, compatibility, wettability, stability, adsorption, etc. ☆ Fatigue testing / tensile strength, temperature dependence, viscoelasticity, elastic modulus, viscosity, stress relaxation, creep, master curve, residual strain, etc.

• Analytical Equipment and Devices

Measurement capabilities offered by TA Instruments ☆ Thermal analysis / glass transition, crystallization, thermogravimetric analysis, curing reactions, expansion rate, thermal conductivity, shrinkage rate, effects of moisture, etc. ☆ Viscoelastic measurements (rheology, rheometers) / viscoelasticity, elastic modulus, viscosity, stress relaxation, creep, master curves, residual strain, molecular weight, molecular weight distribution, etc. ☆ Microcalorimetry / intermolecular interactions, crystallization, amorphousness, aggregation/precipitation, dispersibility, solubility, compatibility, wettability, stability, adsorption, etc. ☆ Fatigue testing / tensile strength, temperature dependence, viscoelasticity, elastic modulus, viscosity, stress relaxation, creep, master curves, residual strain, etc.

• Analytical Equipment and Devices

The viscoelastic measurement device, the "Discovery Hybrid Rheometer," controls the surrounding environment and performs measurements over a wide range of force, strain, and strain rate. We offer three models to meet the needs for sensitivity and capability, from the high-sensitivity HR-30 to the general-purpose HR-10. This product improves various performances and specifications, achieving accurate strain, strain rate, stress control, and normal force, and is equipped with our innovative patented Smart Swap geometry and Smart Swap temperature control system. 【Main Features】 ■ Ultra-low inertia drag cup motor (patented) ■ Magnetic bearings (patented) ■ High-resolution optical encoder ■ Optical encoder dual reader (patent pending) ■ Normal force rebalance transducer (FRT)

• Analytical Equipment and Devices

The DIL 806 optical dilatometer is a high-performance thermal expansion and contraction measurement device provided by TA Instruments. By adopting optical measurement principles, this device enables non-contact measurements that were difficult with conventional dilatometers. The DIL 806 uses an absolute measurement process that is not affected by the expansion or contraction of the testing apparatus itself, eliminating the need to correct measurement results for different temperature programs. This device irradiates a wide planar light onto the sample using high-performance LEDs and detects the shadow of the sample with a high-resolution CCD sensor. A digital edge detection processor evaluates this signal, accurately and sensitively measuring the dimensional changes of the sample in response to temperature variations. The DIL 806 is ideal for measuring materials such as metals and plastics, and thin samples can be easily analyzed using a dedicated sample holder. The furnace allows for rapid heating up to 100°C/min and rapid cooling from 1400°C to 50°C in under 10 minutes. This enables efficient analysis of dynamic processes and tests that include multiple temperature steps.

• Analytical Equipment and Devices

The DIL820 series (DIL 821/822) is a high-precision vertical dilatometer belonging to the DIL 820 series from TA Instruments. These models are equipped with a new optical encoder that has a resolution of 1nm, making them particularly suitable for the analysis of challenging samples. The DIL 822 employs true differential measurement technology, providing the best sensitivity and accuracy for CTE (coefficient of thermal expansion) in the market.

• Analytical Equipment and Devices

The DIL 803 is a dual-sample dilatometer that maximizes productivity by measuring two samples simultaneously. It can measure in vacuum or inert gas environments, while the DIL 803L is specialized for measurements in air. The horizontally arranged furnace ensures uniform temperature and eliminates the effects of air convection. A high-sensitivity LVDT is used to accurately measure even minute thermal expansion events.

• Analytical Equipment and Devices

The DIL 802 is a device that achieves true differential measurement, providing the highest measurement accuracy. By measuring only the difference between the sample and the reference material, it eliminates the effects of system expansion. This design is particularly beneficial for dynamic temperature programs and measurements at low temperatures. The DIL 802 is suitable for measurements in vacuum or inert gas, while the DIL 802L is specialized for measurements in air. The horizontally arranged furnace ensures temperature uniformity and eliminates the effects of air convection. A high-sensitivity LVDT is used to accurately measure even minute thermal expansion events.

• Analytical Equipment and Devices

The DIL 801 is an ideal device for measuring the thermal expansion of a single sample. It allows measurements in vacuum or inert gas environments, while the DIL 801L is specialized for measurements in air. This makes it suitable for evaluating the properties of ceramic materials. The horizontally arranged furnace ensures temperature uniformity and eliminates the effects of air convection. A high-sensitivity LVDT is used to accurately measure even minute thermal expansion events. Key features: - Measurement of linear dimensional changes over a wide temperature range - Capable of measurements in vacuum, inert gas, and air - Accurate displacement measurement with high-sensitivity LVDT - Ensures temperature uniformity with a horizontally arranged furnace - Compatible with various furnaces and easily interchangeable - Accurate temperature measurement with thermocouples or pyrometers - The measurement system can be composed of materials such as quartz glass, alumina, sapphire, graphite, and tungsten.

• Analytical Equipment and Devices

Data Content This is a PDF version of the lecture materials from YouTube, converted for easier viewing. The video consists of a total of 14 pages and provides easy-to-understand explanations for beginners on the following topics related to DSC: - Glass transition - Crystalline polymers - Temperature-modulated DSC (MDSC) I think it might be difficult to understand with just the lecture materials, so please also refer to the YouTube videos below. YouTube TA Summary Site: https://www.youtube.com/channel/UCk3XzqRdsNQz1hJlqKrfujQ DSC Basics Part 3: https://www.youtube.com/watch?v=wWE7fOx7hD4

• Analytical Equipment and Devices

Data Content This is a PDF version of the lecture materials from YouTube, converted for easier viewing. The video consists of a total of 12 pages and provides easy-to-understand explanations for beginners on the following topics: - Rheology of dispersed systems - Emulsions - Carbon black-containing materials I think it may be difficult to understand just from the lecture materials, so please also refer to the YouTube videos below. YouTube TA Summary Site: https://www.youtube.com/channel/UCk3XzqRdsNQz1hJlqKrfujQ Rheology Basics Part 3: https://www.youtube.com/watch?v=VmGG8yTRs8Q

• Analytical Equipment and Devices

Data Content This is a PDF version of the lecture materials from YouTube, converted for better readability. The video consists of a total of 12 pages and provides easy-to-understand explanations for beginners on the following topics related to DSC: - What is a flow curve? - Weissenberg effect - Thixotropic I think it might be difficult to understand with just the lecture materials, so please also refer to the YouTube videos below. YouTube TA Summary Site: https://www.youtube.com/channel/UCk3XzqRdsNQz1hJlqKrfujQ Rheology Basics Part 2: https://www.youtube.com/watch?v=P3BxRkHnQ8w

• Analytical Equipment and Devices

Data Content This is a PDF version of the lecture materials from YouTube, converted for better readability. The video consists of a total of 12 pages and provides easy-to-understand explanations for beginners on the following topics: - What is rheology? - What is viscoelasticity? - About measurement modes. I think it might be difficult to understand just from the lecture materials, so please also refer to the YouTube videos below. YouTube TA Summary Site: https://www.youtube.com/channel/UCk3XzqRdsNQz1hJlqKrfujQ Rheology Basics Part 1: https://www.youtube.com/watch?v=_gPrWIK6yYo&t=4s

• Analytical Equipment and Devices

We have provided a list of various polymer materials used in DSC analysis along with their melting heats.

• Analytical Equipment and Devices

TA Instruments continues to be the leading company in the world of DSC with innovative and outstanding technology. It provides reliable data and enhances workflow and productivity in laboratories. The Nano DSC is a differential scanning calorimeter (DSC) that can detect minute heat changes associated with the conformational changes of biomolecules. Characterization of materials is essential at all stages of product design, manufacturing, processing, and application. Differential scanning calorimeters/nano DSCs are the most widely used thermal analysis instruments for the physical property evaluation of a broad range of materials, including polymers, pharmaceuticals, food, biomaterials, organic compounds, inorganic compounds, and composites.

• Analytical Equipment and Devices

Data Content This is a PDF version of the lecture materials from YouTube, converted for easier viewing. The video consists of a total of 13 pages and provides an easy-to-understand explanation for beginners about DSC, including: - Glass transition - Crystalline polymers - Temperature-modulated DSC (MDSC) I think it may be difficult to understand with just the lecture materials, so please also refer to the YouTube video below. YouTube TA Summary Site: https://www.youtube.com/channel/UCk3XzqRdsNQz1hJlqKrfujQ

• Analytical Equipment and Devices

Data Content This is a PDF version of the lecture materials from YouTube, converted for easier viewing. The video consists of a total of 12 pages and provides an easy-to-understand explanation for beginners about: - Principles - Analytical methods - Enthalpy relaxation (recovery) I think it might be difficult to understand with just the lecture materials, so please also refer to the YouTube videos below. YouTube TA Summary Site: https://www.youtube.com/channel/UCk3XzqRdsNQz1hJlqKrfujQ DSC Basics Part 1: https://www.youtube.com/watch?v=DbGpordpweg

• Analytical Equipment and Devices

The DSC measurements conducted with microscope accessories provide insights through multiple applications to better understand the properties and behaviors of materials. It is possible to capture images related to crystallization and melting transitions, flow of materials above the glass transition and melting points, phase transitions, and volume dimensional changes associated with evaporation and sublimation. Visual observation of color changes and other appearance alterations is used in combination with DSC data to gain a deeper understanding of the material being analyzed.

• Color camera

The calorimetry measurement device (TAM series) is an instrument known as a microcalorimeter that measures very small amounts of heat. By combining a thermostat with high isothermal performance with a calorimeter (calorimeter) suited to the sample and measurement method, it is possible to measure minute heat generated or consumed during physical processes or chemical reactions with sensitivity exceeding microwatts. It is a useful tool that can contribute to the research and development of biofuels and environmental improvement, allowing real-time calorimetry measurements while performing operations such as the addition, mixing, and titration of chemicals through module combinations. This document provides a detailed explanation of high-sensitivity calorimetry measurements of biofuels, which are difficult to observe with conventional differential scanning calorimeters (DSC), as well as real-time measurements of heat changes associated with chemical reactions. ◇ Quantification of wax based on the heat of solidification reactions ◇ Evaluation of the production rate of biofuels *Please download the document.

• Analytical Equipment and Devices

◆Vibration Absorption and Viscoelastic Properties of Polyolefin-based Materials Materials with vibration absorption properties are attracting attention as they enable improvements in labor and living environments through soundproofing and vibration isolation. It is believed that vibration absorption occurs due to energy loss associated with internal friction in the material, and the amount of energy loss is known to correlate with the material's viscoelastic properties. By conducting viscoelastic measurements of the material, information regarding vibration absorption can be obtained. ◆Measurement and Control of Residual Solvent Levels in Wire Coating Processes Insulated wires used in discrete wiring circuit boards can cause various product defects (blisters, delamination, etc.) due to residual solvents present in the wire coating material. However, by utilizing thermal analysis techniques for the detection and quantification of residual solvents, it is possible to implement high-precision quality control.

• Analytical Equipment and Devices

As the industrial sector has begun to focus more on developing and manufacturing environmentally friendly products, various new biodegradable polymers have been adopted. Poly(Lactic Acid) (PLA) is a biodegradable aliphatic polyester produced from lactic acid obtained through the saccharification and fermentation of starch. Due to its high mechanical strength comparable to PETE and good biocompatibility, PLA has been commonly used in biomedical applications such as sutures and stents, but the expansion of PLA's applications is being considered. Understanding the properties of PLA is essential for the development of new applications. We present materials that investigate the thermal and mechanical properties of PLA-based beverage cups using temperature-modulated DSC and DMA. *Please download the materials.

• Analytical Equipment and Devices

Currently, the novel coronavirus infection (COVID-19) is a global issue. TA Instruments hopes to contribute, even in a small way, to addressing the challenges posed by COVID-19 by introducing examples of virus research conducted by universities and research institutions using TA equipment. Research institutions that incorporate studies using Differential Scanning Calorimetry (DSC) and Isothermal Titration Calorimetry (ITC) to understand the structure and mechanisms of viruses are rapidly advancing. Please take a look at the examples.

• Analytical Equipment and Devices