Chemical Analysis Concierge Service

Sample 1, including comparison with Ref! Summarize and conduct candidate analytical methods.

We would like to introduce our "Chemical Analysis Concierge Service." When conducting component analysis of foreign substances or stains on products, it can be challenging to determine whether organic analysis or inorganic analysis is more suitable, and which specific analysis method within organic or inorganic analysis is the best fit. We provide a comprehensive service for customers who are struggling with the selection of analysis methods. Since each analytical instrument can measure different targets, it is necessary to choose a method that aligns with your objectives based on the information available. 【Features】 ■ Reporting only the data for which results have been obtained ■ Results report can include up to 2 methods ■ If you wish to receive results for more than 3 methods, additional costs will apply *For more details, please refer to the PDF document or feel free to contact us.

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If it is 5 micrometers or larger, foreign object IR data can be obtained.

■Service Overview 1. Micro ATR Method IR data acquisition of foreign substances is possible if they are approximately 5um or larger. 2. Surface Distribution Image Observation of the in-plane distribution of organic substances is possible. 3. Temporal Changes Measurement of the state of organic substances that change on a second-by-second basis is possible.

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We will report rapid analysis results using various sampling techniques regarding foreign substances that significantly impact the yield of electronics products.

■Special Sampling Techniques for Foreign Substances in Multilayer Films - Foreign substances buried in metal films on substrates Metal film etching ⇒ Transfer to Si wafer ⇒ FT-IR analysis - Foreign substances in multilayer films Cutting off the surface layer ⇒ Transfer to Si wafer ⇒ FT-IR analysis Microtome/FIB thinning ⇒ Transfer to Si wafer ⇒ FT-IR analysis

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TOF-SIMS can analyze light elements and inorganic substances as well as large organic molecules.

■TOF-SIMS Three Analysis Modes - High-resolution mass spectrum - Depth profile analysis - Surface mapping analysis

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We conduct surface analysis, foreign substance analysis, and organic composition analysis.

At AITES, we propose and conduct contract analysis menus suitable for the purpose and sample, including the analysis of organic and inorganic substances, foreign substances, and surface analysis. In this department, we perform component analysis of microscopic foreign substances using advanced sampling techniques, as well as impurity analysis in samples, conducting both qualitative and quantitative analysis of organic and inorganic components. Additionally, we analyze the surface of samples for contamination and oxidation states. 【Service List】 ■ Component analysis of epoxy resin curing agents using Pyrolysis GC/MS ■ Analysis of microscopic organic foreign substances using Imaging FT-IR ■ Analysis of microscopic foreign substances using Micro-Raman spectroscopy ■ Ion Chromatography (IC) analysis, etc. *For more details, please refer to the PDF document or feel free to contact us.

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Introducing a new device! We present an analytical method aimed at the qualitative and quantitative analysis of components contained in samples.

We have introduced the "GC-MS Gas Chromatograph Mass Spectrometer" manufactured by Shimadzu Corporation. This is one of the analytical methods aimed at qualitative and quantitative analysis of components contained in samples, used for the qualitative and quantitative analysis of volatile organic compounds such as parts, materials, residual solvents, and additives. It is necessary for the measurement target to be gasified (with a boiling point below 300°C), but it is suitable for component analysis of mixtures due to its higher sensitivity compared to IR and RAMAN, as well as the ability to separate components in the GC section. 【Overview of GC-MS Equipment】 ■ GC-MS Main Unit: GC-2030, GCMS-QP2020 NX ■ Headspace Sampler: HS-20 ■ Pyrolysis Analyzer: Multi-Shot Pyrolyzer Py-3030 ■ Specifications ・Detection Limit: Several ppm (varies depending on the measurement target) ・Headspace: 40–300°C, Sample Size 13mm x 40mm or smaller ・Pyrolysis Analyzer: 50–1050°C (EGA measurement compatible), Sample Size up to 4mm *For more details, please refer to the PDF document or feel free to contact us.

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We offer a variety of measurement modes, including double cantilever beam bending and three-point bending with free support!

"DMA (Dynamic Mechanical Analysis)" is an analysis method that applies periodic oscillatory loads to polymer materials and measures the resulting stress and phase difference to determine elasticity and viscosity as a function of temperature. It provides information related to molecular motion and molecular structure of polymers, such as glass transition and relaxation. 【Features】 ■ Dynamic mechanical analysis ■ Applies periodic oscillatory loads to polymer materials ■ Measures elasticity and viscosity as a function of temperature ■ Obtains information related to molecular motion and molecular structure of polymers ■ Multiple measurement modes *For more details, please refer to the PDF document or feel free to contact us.

• Weight related measuring instruments
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Observe the degree of endothermic/exothermic reaction of the sample! The temperature range is possible from -90°C to 550°C.

DSC (Differential Scanning Calorimetry) is an analytical method that determines the difference in heat flow between a sample and a reference material as a function of temperature changes in the sample, allowing for the observation of the degree of endothermic/exothermic reactions in the sample. The temperature range is -90°C to 550°C, the required sample amount is 5 to 10 mg, and the sample shapes that can be measured include films, powders, and bulk materials. 【Features】 ■ Differential Scanning Calorimetry ■ Observation of the degree of endothermic/exothermic reactions in the sample ■ Temperature range: -90°C to 550°C ■ Required sample amount: 5 to 10 mg ■ Sample shapes: films, powders, bulk *For more details, please refer to the PDF document or feel free to contact us.

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Output the temperature difference between the sample and the reference material as a DTA signal! Change the temperature according to a constant program.

TG-DTA (Thermogravimetric Differential Thermal Analysis) is an analysis that simultaneously measures the weight of a sample (TG) and the temperature difference between the sample and a reference material (Differential Thermal Measurement) (DTA) as a function of temperature, while varying the sample's temperature according to a specific program. The measurable conditions are a temperature range of room temperature to 1000°C, a required sample amount of 10 to 20 mg, and sample shapes including film, powder, and bulk. 【Features】 - Thermogravimetric Differential Thermal Analysis - Varies the sample's temperature according to a specific program - Simultaneously measures the sample's weight and the temperature difference from the reference material as a function of temperature - Required sample amount: 10 to 20 mg - Sample shapes include film, powder, and bulk *For more details, please refer to the PDF document or feel free to contact us.

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Information on thermal expansion, thermal contraction, and glass transition temperature can be obtained in multiple measurement modes!

TMA (Thermomechanical Analysis) is a method that measures the dimensional changes of a sample while applying a constant load and varying the sample temperature. It provides information on thermal expansion, thermal contraction, glass transition temperature, and more. The temperature range is from -150 to 1000°C, with a maximum size of Φ10×25mm (compression mode, needle insertion mode) and a maximum size of 0.7mm×5mm×20mm (tensile mode) as measurable conditions. This document includes case studies of TMA analysis for semiconductor encapsulants. 【Features】 ■ Thermomechanical measurement ■ Applying a constant load to the sample while varying the sample temperature ■ Measuring the dimensional changes of the sample ■ Obtaining information on thermal expansion, thermal contraction, glass transition temperature, etc. ■ Multiple measurement modes *For more details, please refer to the PDF document or feel free to contact us.

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As an example of organic matter analysis, I would like to introduce a case where polyethylene glycol was analyzed.

TOF-SIMS can detect elements and organic molecules, as well as fragment ions, making it effective for organic analysis. As an example of organic analysis, we will introduce a case study of polyethylene glycol. Secondary ion mass spectra can provide valuable insights for the qualitative analysis of organic substances. In this case study, we can confirm the characteristic repeating structure of polyethylene glycol (C2H4O) as a peak group with a mass difference of 44. Calculating from the mass number, it is inferred that the terminal groups are H- and HO-, suggesting they are detected as protonated species. *For more details, please refer to the PDF document or feel free to contact us.*

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The analysis sensitivity of TOF-SIMS is high at the ppm level, making it effective for analyzing trace contamination!

This is an introduction to a case where water droplet-shaped contaminants were created on a Si wafer through reproducibility experiments. Measurements were conducted at the same position using SEM-EDX and TOF-SIMS, and a comparison of the image maps was made. In the TOF-SIMS image map, organic substances (CH, CN), Na, and K were detected around the watermark. While no contaminants were observed around the watermark in the optical image, SEM image, and EDX analysis, the TOF-SIMS image map revealed that trace amounts of contaminants were present. *For more details, please refer to the PDF document or feel free to contact us.*

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By using micro-Raman, it is possible to evaluate the crystallinity in a fine range (1μm and above)!

At Aites Co., Ltd., we offer analysis and reliability evaluation services for "Crystallinity Analysis of Resin Materials using Micro-Raman Spectroscopy." Using the spectra obtained from a micro-Raman spectrophotometer, it is possible to determine the crystallinity of resin materials in fine detail based on the differences in the half-width of the peaks. We also have analysis cases that investigate the changes in crystallinity from the mouth of PET bottles to the bottle body. Please leave the analysis, evaluation, and reliability assessment to us. [Overview] ■ Crystallinity Analysis of Resin Materials using Raman Spectroscopy - The linewidth of the Raman spectrum changes to reflect crystallinity - It is possible to determine the half-width of the C=O stretching band and the crystallinity - It is possible to determine the relative crystallinity of PET *For more details, please refer to the PDF document or feel free to contact us.

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Comparison of components in liquid crystal panels using gas chromatography-mass spectrometry (GC-MS) is published!

This document introduces a comparison of components in PC monitors and digital clocks using gas chromatography-mass spectrometry (GC-MS). Liquid crystal displays contain small organic substances (liquid crystal molecules). These have evolved into molecular structures suitable for product characteristics due to technological innovations. Our company clarifies these differences at the molecular level using GC-MS, allowing us to confirm that the liquid crystal molecules are appropriate for their intended use and to check for the presence of impurities. [Contents] ■ Component comparison of PC monitors and digital clocks using GC-MS ■ Case studies of GC-MS analysis of liquid crystal components We compared the number of components and characteristics of segment-type liquid crystal displays (digital clocks) and color TFT liquid crystal displays (PC monitors). *For more details, please refer to the PDF document or feel free to contact us.

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Depth-direction measurements using Raman spectroscopy! Material analysis of each layer is possible from the surface of multilayer films.

Our "Micro Raman Spectrophotometer" employs a confocal optical system, allowing for the adjustment of the focal position in the depth direction, similar to a microscope, enabling material analysis of each layer from the surface of multilayer films. Using the confocal function of the micro Raman spectrophotometer, the focus of the Raman laser light can be varied in the depth direction. Additionally, by continuously changing the focal position, it is possible to obtain spectra continuously in the depth direction. 【Features】 ■ Adoption of a confocal optical system ■ Enables material analysis of each layer from the surface of multilayer films ■ Capable of varying the focus of the Raman laser light in the depth direction ■ Allows for continuous spectral acquisition in the depth direction *For more details, please refer to the PDF document or feel free to contact us.

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What is the reason for this discoloration on the surface? Why are there cracks in such places? These issues will be resolved from the perspectives of electrons, atoms, molecules, and chemical reaction mechanisms!

Many defects occur during the manufacturing process of products and during their use. Among these, there are challenges related to material properties, and for those who are wondering, "It’s probably due to the material, but what should I do about it?", we propose solutions from the perspectives of electronics, atoms, molecules, and chemical reaction mechanisms. ■Examples of Challenges - What is causing this discoloration? - Why did it crack so quickly? - Why does it break immediately when subjected to a tensile test? *For more details, please refer to the PDF document or feel free to contact us.

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Non-destructive depth analysis of thin films on the nm order is possible! We will also introduce analysis examples.

At Aites Co., Ltd., we conduct depth profile analysis of thin film layers using angle-resolved XPS. By changing the angle between the sample and the XPS photoelectron detector, it is possible to vary the detection depth of the photoelectrons. The data obtained from this is numerically analyzed through simulation and converted into a depth profile. We achieve depth profile analysis of uniform thin films in the nanometer order near the surface, which is difficult to measure using conventional ion etching methods. We also have examples of analyzing the depth profile of HDD magnetic surfaces. 【Features】 ■ Non-destructive depth profile analysis of thin films in the nanometer order is possible ■ Achieves depth profile analysis of uniform thin films *For more details, please refer to the PDF document or feel free to contact us.

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Clear publication of analysis results using polyamide imide materials and IR devices, as well as data analysis!

This document introduces a case study that clarifies the causes of discoloration in super engineering plastic polyamide-imide (PAI) films used in coatings, composite film materials, and various molded products through equipment analysis and reaction mechanisms. It includes analysis results from IR equipment, data analysis, and reaction mechanisms, starting with the material polyamide-imide. While the storage stability of the raw materials used in product manufacturing is essential, environmental conditions during the processing can sometimes induce defects. We encourage you to read it. [Contents] ■ About the material polyamide-imide ■ Analysis results from IR equipment ■ Data analysis and reaction mechanisms *For more details, please refer to the PDF document or feel free to contact us.

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Analysis of inorganic compounds such as metal oxides is also possible!

The corrosion process of iron involves various compounds depending on the degree of corrosion, and even the same iron oxides and hydroxides exhibit different spectra due to differences in valence and crystal structure. Raman analysis allows for the confirmation of the oxidation state of iron in a micron-order fine range. [Analysis Content] ■ Analysis of rust formed on the iron surface - A mixture of FeOOH and Fe2O3 - A mixture of FeOOH, Fe3O4, and Fe2O3 ■ Raman spectrum of iron rust components *For more details, please refer to the PDF document or feel free to contact us.

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Analysis of inorganic compounds such as metal oxides is also possible! We will introduce the analysis of black spots on the surface of copper-clad laminates.

We would like to introduce a case where discoloration on the surface of a copper-clad laminate was analyzed using Raman spectroscopy. Our Raman spectral analysis can analyze not only organic substances but also inorganic compounds such as metal oxides. Please feel free to contact us when needed. [Analysis Details] ■ Analysis of black spots on the surface of the copper-clad laminate - Slight discoloration is observed on the surface - Upon magnification, a condition resembling black stains is seen - A spectrum of CuO was obtained from the discolored area - The nature of the discoloration is believed to be copper oxide formed on the surface of the copper *For more details, please refer to the PDF document or feel free to contact us.

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We will introduce a case that elucidates the differences in linear expansion coefficients of PET and PEN films with similar main skeletal structures and the mechanisms that produce these differences.

Although they are different materials, if they have similar molecular structures, there is potential for the development and expansion of composite products due to their compatibility and similar properties. However, while they are similar, there are also pitfalls. For example, differences in linear expansion rates can cause strain and displacement at their interface, leading to delamination in many cases. This document presents a case study that clarifies the differences in linear expansion rates between PET and PEN films, which have similar main chain structures, and the mechanisms that produce these differences. [Contents] - About materials PET and PEN - XPS analysis (comparison of bonding states) - TMA analysis (comparison of linear expansion rates) - Data analysis *For more details, please refer to the PDF document or feel free to contact us.

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Detection of certain organic substances is possible! Here is an example of measuring low molecular weight organic acids in an anion exchange mode.

This document presents case studies on the analysis of low molecular weight organic acids using ion chromatography. In ion chromatography, it is possible to detect some organic substances in addition to Cl-, Br-, and SO4^2-. As an analysis case, we will show an example of measuring low molecular weight organic acids in an anion exchange mode. We invite you to read it. 【Published Cases】 ■ Lactic acid, acetic acid, propionic acid, formic acid ■ Acrylic acid, methacrylic acid ■ Benzoic acid *For more details, please refer to the PDF document or feel free to contact us.

• Analytical Equipment and Devices
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It is possible to monitor the progress of the adhesive curing reaction (degree of curing)!

FT-IR spectra sensitively reflect the bonding states of organic materials, making it possible to monitor the progress of adhesive curing reactions (degree of curing). The procedure for measuring the degree of curing of the resin involves comparing the spectra of unreacted materials with those of materials after 100% reaction to identify the changing regions. The degree of curing for unreacted materials is set at 0%, and that for reacted materials is set at 100%. The peak intensity of the measurement sample spectrum is interpolated to determine the reaction rate (degree of curing). 【Procedure for Measuring Degree of Curing】 ■ Compare the spectra of unreacted materials with those of materials after 100% reaction to identify the changing regions. ■ Set the degree of curing for unreacted materials at 0% and that for reacted materials at 100%. ■ Interpolate the peak intensity of the measurement sample spectrum to determine the reaction rate (degree of curing). *For more details, please refer to the PDF document or feel free to contact us.

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Sampling using capillaries through surface tension! FT-IR analysis has become possible.

Traditionally, sampling of liquid foreign substances has been considered very difficult. In the liquid foreign substance sampling technique for FT-IR analysis, sampling is performed using a capillary and surface tension, making FT-IR analysis possible. 【Sampling Procedure】 ■ Liquid foreign substances on the substrate ■ Sampling with a capillary ■ Transferring the liquid onto a Si wafer for FT-IR analysis ■ Sampling in progress with the capillary ■ Transferring to the Si wafer *For more details, please refer to the PDF document or feel free to contact us.

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Solid samples can leach ionic components into pure water! Trace ionic components in the aqueous solution can be detected with high sensitivity.

"Ion Chromatography Analysis" allows for qualitative and quantitative analysis of trace ionic components in aqueous solutions. Separation is performed using a column filled with ion exchange resin, and by measuring electrical conductivity, trace ionic components in aqueous solutions can be detected with high sensitivity. Solid samples are dissolved in pure water to measure the ionic components. 【Main Specifications】 ■ Anions: Cl-, Br-, NO2-, NO3-, organic acids, etc. ■ Cations: Li+, Na+, K+, Mg2+, Ca2+, etc. ■ Quantification limit: Approximately 100 ppb (varies by ion species) ■ Detection limit: Approximately 10 ppb (varies by ion species) ■ Detector: Electrical conductivity (suppressor type) *For more details, please refer to the PDF document or feel free to contact us.

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Introducing a method for analyzing near the surface through total internal reflection of infrared light by closely adhering micro ATR crystals!

Based on imaging obtained from FT-IR spectra using the ATR method, cross-sectional analysis of organic multilayer films such as aluminum laminate film can be performed. The ATR method (Attenuated Total Reflection) is a technique that involves closely adhering a micro ATR crystal to the sample, allowing for analysis near the surface through total internal reflection of infrared light. Due to the influence of the refractive index of the crystal applied to the sample, the apparent spatial resolution is enhanced, enabling the analysis of smaller foreign substances. 【Features of the ATR Method】 ■ A technique that analyzes near the surface through total internal reflection of infrared light ■ Enhanced apparent spatial resolution due to the influence of the refractive index of the crystal applied to the sample ■ Enables the analysis of smaller foreign substances *For more details, please refer to the PDF document or feel free to contact us.

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It is possible to investigate the layer structure of organic films! Introducing imaging FT-IR analysis of high-performance multilayer film cross-sections.

It is possible to investigate the layer composition of organic films using FT-IR imaging through transmission of organic multilayer membranes that have been sectioned with a microtome. The document introduces imaging FT-IR analysis of high-performance multilayer film cross-sections using photos and graphs. [Imaging FT-IR Analysis of High-Performance Multilayer Film Cross-Sections] ■ Sample: High-performance multilayer film ■ Measurement Area: Transmission/Reflection method 175μm, ATR method 35μm ■ Spatial Resolution (Pixel Size): Transmission/Reflection method 5.5μm, ATR method 1.1μm *For more details, please refer to the PDF document or feel free to contact us.

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By adding a special reagent to the sample and heating it, it becomes possible to detect substances that are usually difficult to detect!

In a typical thermal decomposition GCMS, samples are heated to detect volatile components; however, analyzing components that do not volatilize upon heating or those with low detection sensitivity is challenging. Therefore, by adding a special reagent to the sample and heating it, it becomes possible to detect substances that are usually difficult to identify. For example, in the analysis of polymers, thermal decomposition of the polymer results in the detection of a large number of decomposition products, and in some cases, peaks may overlap with other additives, making analysis difficult. However, by performing reactive thermal decomposition GCMS, it is possible to detect the methyl esters of monomers and to separate and analyze them from the additives. Thus, even when the target analytes are difficult to detect using conventional analysis, reactive thermal decomposition GCMS allows for sensitive detection by selecting appropriate reagents for the analytes. [Examples] - Analysis of phthalate esters (DIDP) - Analysis of polymers (polyethylene terephthalate) - Analysis of copper corrosion inhibitors (BTA) *For more details, please refer to the PDF document or feel free to contact us.

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We will suggest appropriate analysis methods based on the condition of polymer materials and samples!

At AITES Co., Ltd., we conduct material degradation analysis. We propose appropriate analytical methods based on the condition of polymer materials and samples. By analyzing the degradation process that the material has undergone and optimizing the polymer materials and usage environment, it is possible to extend the product's lifespan. *For more details, please refer to the PDF document or feel free to contact us.

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Distinguish and identify compounds with similar structures! You can obtain information such as the number of protons and structural characteristics.

At Aites Co., Ltd., we conduct 1H NMR analysis of phthalate esters. NMR analysis and GCMS analysis are effective for distinguishing and identifying compounds with similar structures. In this analysis, we can obtain information about the number of protons from the integral values, structural features such as functional groups from the chemical shifts, and the positional relationships with surrounding protons from the coupling patterns and coupling constants. *For more details, please refer to the PDF document or feel free to contact us.

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Distinguish compounds with similar molecular structures through NMR analysis, elucidating the binding positions of side chains and substituents, as well as branching structures!

At Aites Co., Ltd., we conduct 1H NMR analysis of phthalate esters. NMR analysis is an effective method for distinguishing compounds with similar molecular structures and elucidating structures such as the bonding positions of side chains and substituents, as well as branching structures. In organic synthesis and polymer synthesis, it is an essential analysis to confirm whether the desired molecular structure has been obtained. The characteristic effects and efficacy of pharmaceuticals, supplements, food, and fibers are influenced by the positions of substituents in the molecular group and the molecular structure. Our skilled team will provide in-depth organic molecular structure analysis. *For more details, please refer to the PDF document or feel free to contact us.

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Publication of headspace GC-MS analysis method and case study of outgassing component analysis of liquid crystal panel polarizers!

If solvents, low molecular organic substances, or unreacted materials remain in the constituent materials, packaging materials, or cushioning materials of a product, they may outgas, diffuse, or permeate into the constituent materials, potentially affecting the product's lifespan, characteristics, and the environment or human health. The headspace method of GCMS is effective for qualitative and quantitative analysis of trace residual substances. This document presents a case study of the qualitative analysis of outgassing components from polarizers used in liquid crystal panels. We encourage you to read it. [Contents] ■ Headspace GC-MS analysis method ■ Analysis of outgassing components from polarizers in liquid crystal panels *For more details, please refer to the PDF document or feel free to contact us.

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It will lead to the determination of development direction and acceleration! We will respond with abundant technology, knowledge, and equipment.

In research and development, analysis and evaluation are essential processes that serve as checkpoints, and the materials that make up the product often become key subjects of focus. Aites assists manufacturers in their research and development with a diverse range of analytical instruments, observation devices, reliability testing equipment, and accumulated knowledge and chemical reaction mechanisms. We are ready to support you with our extensive technology, knowledge, and equipment, so please feel free to contact us. 【Features】 <Examples of Analytical Instruments> ■ Microscopic IR ■ Microscopic Raman ■ (EGA/TD/Pyr) GC-MS ■ TOF-SIMS *For more details, please refer to the PDF document or feel free to contact us.

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Examples of degradation analysis of panel polarizers are published! We conducted degradation analysis through reliability testing and outgassing analysis using HS-GCMS.

The polarizers used in LCD panels are made of multilayer films laminated with materials such as triacetyl cellulose, polyvinyl alcohol, and polyethylene terephthalate. This document presents a case study of the degradation analysis of panel polarizers after reliability testing, conducted through HS-GCMS analysis and thermal desorption GCMS analysis. Even invisible degradation might be detected with this analysis?! Please take a moment to read it. [Contents] ■ Reliability Testing ■ Outgassing Analysis via HS-GCMS ■ Low Boiling Point Component Analysis via Thermal Desorption GCMS *For more details, please refer to the PDF document or feel free to contact us.

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Detect and analyze the absorption wavelengths of organic molecular groups (functional groups)!

At Aites Co., Ltd., we conduct "FT-IR analysis" to confirm the degradation of resins. The degradation of resins can manifest as visible discoloration or invisible changes. Discoloration can be detected through visual changes, but invisible changes can lead to a decrease in strength and become the source of various issues. IR analysis allows us to understand the changes in molecular structure caused by these alterations. *For more details, please refer to the PDF document or feel free to contact us.*

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Introducing a case where the changes in molecular structure of materials were verified through IR analysis! We also creatively accommodated a variety of sample setups.

Reliability testing of materials that make up the product under thermal and humidity loads is essential, but analysis and evaluation after testing is also an indispensable process. Constant temperature and humidity testing is a device that applies temperature and humidity loads to products and materials to check for changes in physical properties, characteristics, appearance, and lifespan. Our company has also devised various methods for setting up a wide range of samples. In this document, we will introduce a case where changes in the molecular structure of materials before and after constant temperature and humidity testing were verified through IR analysis. We encourage you to read it. [Contents] ■ Examples of reliability testing equipment (constant temperature and humidity testing equipment) ■ Innovations in sample setup ■ Comparative evaluation before and after testing through chemical analysis *For more details, please refer to the PDF document or feel free to contact us.

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Here is an example of analyzing the polymer components and additives used in PTP packaging sheets for tablet packaging!

This document introduces the analysis of PTP packaging sheets through EGA-MS analysis and thermal desorption/pyrolysis GC-MS analysis. Various materials are used in industrial products; for example, polymers contain low molecular weight components such as additives and high molecular weight components that are the polymers themselves. In GCMS analysis, low molecular weight components volatilize at relatively low temperatures, while high molecular weight components need to be decomposed at high temperatures before analysis. Here, we present an example of the analysis of the polymer components and additive components of PTP packaging sheets used for tablets. We invite you to read it. [Contents] ■ Evolved Gas Analysis Method (EGA-MS Analysis) ■ Analysis Examples of PTP Packaging Sheets *For more details, please refer to the PDF document or feel free to contact us.

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Evaluate higher-order structures using analytical methods! Raman analysis is also effective for analyzing polymer structures.

I would like to introduce "Analysis of Polymer Structural Changes." This document includes "Evaluation of Polymer Higher-Order Structures by Raman Spectroscopy" and "Structural Changes of Polymer Chains." The molecular structure of polymers affects their properties, influencing the physical characteristics of polymer products. We evaluated the higher-order structures formed by the aggregation of polymer chains using analytical methods. Please take a moment to read it. [Contents] ■ Evaluation of Polymer Higher-Order Structures by Raman Spectroscopy ■ Structural Changes of Polymer Chains *For more details, please refer to the PDF document or feel free to contact us.

• Other polymer materials

Clarifying the functions, characteristics, and conditions of products and materials. We propose analytical methods tailored to the analysis target and purpose.

Our "Chemical Analysis Service" analyzes various industrial products and materials, such as panel products, semiconductor products, and resin molded products, at the molecular and atomic levels. We clarify their functions, characteristics, and conditions, contributing to solving our customers' challenges. We can propose analytical methods suitable for the material to be analyzed and the purpose of the analysis. Please feel free to consult us. 【Examples of Analysis Content】 ◎ Foreign substances in products ◎ Condition of materials used ◎ Material degradation ◎ Trace components and elements contained in materials ◎ Physical properties of products and materials due to heat

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We will detect and analyze the atomic emission that occurs when an atom returns from an excited state to its ground state!

In ICP emission spectroscopic analysis, it is possible to detect multiple metal elements contained in a sample simultaneously. This document introduces examples of the analysis of trace metal elements contained in liquid crystals. It includes the principles and overview of ICP-AES analysis as well as measurement examples. Please feel free to contact us regarding the sample state or the elements to be analyzed. [Contents] ■ Principles and Overview of ICP-AES Analysis ■ Measurement Example: Qualitative Analysis of Metal Elements in Liquid Crystal Panels *For more details, please refer to the PDF document or feel free to contact us.

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Leave it to us for everything from chemical analysis and physical testing to reliability testing! Introduction to our measurement and evaluation services.

Plastic extrusion/injection molding processing is set according to the heat resistance temperature (melting point Tm) of the raw materials, but due to the degradation and alteration of the materials, there are cases where molding becomes difficult at the specified setting temperature. By checking the melt flow rate (MFR) of plastic raw material pellets or powders, it is possible to determine whether there are any changes compared to conventional products. We present a case where untreated (no load), temperature and humidity load (constant temperature and humidity test), and UV-irradiated PP (polypropylene) were injected and evaluated at a temperature of 230°C and a load of 5kg, so please take a look at the PDF download. [Evaluation Case] ■PP: Polypropylene ■8585: 85°C 85% × 336 hours ■UV: UV irradiation 253.7nm × 336 hours ■Injection time: 10 minutes (converted from 3 minutes) *For more details, please refer to the PDF materials or feel free to contact us.

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We will solve your problems and issues with our expertise and abundant equipment!

The materials that make up the products are diverse, but the performance of the products often hinges on the characteristics of these materials. At AITES, we provide comprehensive support from reliability testing of materials to observation and physical/chemical analysis. This document presents a case study comparing the molecular structure and thermal property changes of plastic materials before and after exposure to ultraviolet light and constant temperature and humidity conditions. [Contents] ■ Constant temperature and humidity testing, and ultraviolet irradiation (Sample: Polyethylene (PE) pellets) ■ Results of IR, Raman, and EGA analysis *For more details, please refer to the PDF document or feel free to contact us.

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Measures and avoidance of issues are possible! We will introduce examples verified through elemental and bonding state analysis.

Materials often undergo changes and discoloration depending on the usage environment. These changes and discoloration can lead to issues with the product's performance and design, but by understanding and clarifying the changes in molecular structure through chemical analysis, it becomes possible to address or avoid these problems. This document presents case studies that have been compared and verified through elemental and bonding state analysis via surface analysis. [Contents] ■ Analysis Samples ■ Elemental Analysis Results by XPS (ESCA) ■ Bonding State Analysis Results by XPS (ESCA) for Polycarbonate ■ Bonding State Analysis Results by XPS (ESCA) for Polyvinyl Chloride *For more details, please refer to the PDF document or feel free to contact us.

• Contract Analysis

Various surface analysis techniques! We will assist you in solving issues such as foreign substances, discoloration, and contamination.

Our company utilizes various surface analysis techniques to assist in resolving issues such as foreign substances, discoloration, and contamination. We conduct a wide range of analyses, from micro-regions to bulk samples, including "EDX," which is energy-dispersive X-ray analysis; "AES," which detects Auger electrons using electron beams; and "XPS," which allows for the analysis of insulators and chemical bonding states. Please feel free to contact us when you need our services. 【Analysis Methods】 ■EDX (EDS): Energy-dispersive X-ray analysis ■AES: Auger electron spectroscopy ■XPS (ESCA): X-ray photoelectron spectroscopy ■TOF-SIMS: Time-of-flight secondary ion mass spectrometry *For more details, please refer to the PDF materials or feel free to contact us.

• Analytical Equipment and Devices
• Spectroscopic Analysis Equipment
• Contract Analysis

Introducing the results of IR analysis on peripheral materials for LCD displays and raw materials (pellets) such as fibers!

PMMA (acrylic), PET (polyethylene terephthalate), and PC (polycarbonate) are utilized in many applications, taking advantage of their characteristic transparency. They are essential materials for industrial products such as peripheral components of liquid crystal displays, protective films for mobile device screens, headlight covers, optical fibers, and textiles. This document presents the results of IR analysis of these raw materials (pellets). [Contents] - Analysis Sample: Characteristics of Ester/Carbonate-based Polymers - IR Spectrum (ATR Method) - Spectrum Comparison (Overlay) - Other Related Analysis Services *For more details, please refer to the PDF document or feel free to contact us.

• Other contract services

Introducing the usage samples along with their characteristics and the degradation analysis results of polarizing films and light diffusion films!

Polarizing films and light diffusion films are used in LCD products and design applications. They can deteriorate due to environmental conditions such as temperature and humidity, which can lead to a decrease in their polarizing and diffusion properties, affecting LCD screens and designs. This document presents case studies analyzing the deterioration caused by temperature and humidity stress using FT-IR. [Contents] - Sample used and its properties - Deterioration analysis results of polarizing films (comparison of IR spectra before and after testing at 70°C and 85% humidity for 1 week) - Deterioration analysis results of light diffusion films (comparison of IR spectra before and after testing at 70°C and 85% humidity for 1 week) - Other available analytical methods *For more details, please refer to the PDF document or feel free to contact us.

• Other contract services

Introducing the results of IR analysis conducted on polystyrene, polyvinyl chloride (PVC), and others!

There are many types of vinyl polymers, and they exhibit various properties depending on the molecular structure of their side chains. Additionally, differences in crystallinity arise from the bonding configuration of these side chains (stereoisomers). In this document, we present the results of IR analysis of representative vinyl polymers, including polyethylene, polypropylene, polystyrene, and polyvinyl chloride (PVC). Aites conducts advanced data analysis based on chemical theory, ensuring that even subtle differences are not overlooked. Please feel free to consult us at any time. 【Contents】 ■ Analysis Sample: Vinyl Polymers ■ IR Spectrum (ATR Method) ■ IR Spectrum Comparison (Overlay) *For more details, please refer to the PDF document or feel free to contact us.

• Contract measurement

It is possible to measure simply using XPS! Please inquire about semiconductors other than oxide-based ones.

At AITES, we conduct "simple measurement of band gaps using XPS." It is possible to simply measure the band gaps of materials or thin films with relatively wide band gaps among semiconductors and insulators using XPS. When measuring the band gap of β-Ga2O3 using the O1s peak, the band gap of this β-Ga2O3 was measured to be approximately 4.9 eV, based on the difference between the peak position of O1s and the energy loss edge due to the band gap. 【Features】 ■ Can be easily measured using XPS ■ Simple measurement of thin films with wide band gaps, such as SiON, is also possible ■ Supports semiconductors other than oxide-based materials *For more details, please refer to the PDF document or feel free to contact us.

• Contract measurement

Solve the cause of the problem from a chemical perspective! Introducing methods to approach it through chemistry and reaction mechanisms.

Various defects such as cracks, discoloration, delamination, deformation, and reduction in material strength can occur in products and components. Many of these issues are often caused by the materials that make up the products, and analyzing these materials can sometimes lead to solutions. This document introduces an approach to understanding what is happening through chemistry and reaction mechanisms. [Contents] ■ Cracks (breaks), delamination ■ Discoloration, deformation ■ Chemical reaction mechanisms (example of epoxy resin curing) *For more details, please refer to the PDF document or feel free to contact us.

• Contract Analysis

Detect the mass number as an absolute value! You can obtain information about the composition of the compound.

We conduct "pigment and polymer analysis using MALDI-TOFMS." With "MALDI-TOFMS," it is possible to obtain molecular weight information for insoluble substances such as pigments, molecular weight information for synthetic polymers, and information on terminal groups. Please feel free to contact us for mass confirmation of synthetic compounds or for structural analysis in combination with other analytical methods. 【Features】 ■ Adoption of Matrix-Assisted Laser Desorption Ionization Mass Spectrometry (MALDI) ■ Ability to obtain information regarding the composition of compounds ■ Suitable for analyzing polymers that are small compared to GPC and large compared to LCMS ■ Mass numbers are detected as absolute values *For more details, please refer to the PDF document or feel free to contact us.

• Contract measurement
• Contract Inspection

We will elucidate the characteristics at the molecular level using our FT-IR and thermal decomposition GC-MS!

At AITES, we are conducting a structural analysis of Nylon 6.10. Nylon possesses flexibility and a texture similar to silk, while also having high strength and durability that natural fibers do not have, described as "stronger than steel and finer than a spider's silk." We will elucidate these characteristics at the molecular level using our FT-IR and pyrolysis GC-MS. 【Nylon 6.10 Interfacial Polymerization Reaction Mechanism】 1. Electron withdrawal by chlorine leads to a deficiency of electrons in adjacent carbon. 2. The non-bonding electrons of the amine attack the carbon as a nucleophile. 3. The oxygen atom is activated to form an unstable intermediate. 4. Hydrogen chloride is eliminated, forming an amide bond. 5. Interfacial polymerization progresses, resulting in polymerization. *For more details, please refer to the PDF document or feel free to contact us.

• Contract Analysis

It is possible to detect with high sensitivity! We will introduce a case comparing the analysis of Li using TOF-SIMS and SEM-EDX.

We will introduce a case comparing the analysis of lithium (Li) using TOF-SIMS and SEM-EDX. While SEM-EDX is used for the analysis of contamination and foreign substances, it is difficult to detect Li with general EDX, excluding windowless EDX. On the other hand, TOF-SIMS can detect Li with high sensitivity. Please feel free to contact us if you need assistance. 【Overview】 ■ Analysis of stains on copper plates ■ SEM-EDX analysis → Difficult to detect Li ■ TOF-SIMS analysis → Li detectable *For more details, please refer to the PDF document or feel free to contact us.

• Contract measurement

By evaluating the orientation, strain, and birefringence of the material, you can understand the internal stress and strain state!

The materials that make up the product are varied, but if there is significant or uneven internal stress during the manufacturing process, it can lead to issues such as deformation, cracking, and reduced performance due to usage and environmental conditions. By using 'WPA (Wide Polarization Analysis)', it becomes possible to understand internal stress and strain states by evaluating the orientation, strain, and birefringence of the material. Please feel free to consult with us. 【Features】 ■ Ability to understand internal stress and strain states ■ Clarification of material strain and birefringence from a molecular perspective ■ Analysis of defects and theories through multiple methods in a matrix - Raman spectroscopy (qualitative/strain/crystallinity), XRD (X-ray diffraction), AFM/SEM/TEM (crystal structure observation), DSC (degree of crystallization), etc. *For more details, please refer to the PDF document or feel free to contact us.

• Contract Analysis
• Other contract services

Analyze subtle spectral differences using FT-IR! We can also accommodate reliability tests combined with high temperature, cold heat, and more.

Polyethylene resin is a versatile plastic that is commonly found and used in many applications. Depending on the application, the reaction processes (synthesis/polymerization) differ, such as soft types and hard types. Due to the differences in synthesis/polymerization, it is divided into low-density polyethylene (LDPE) and high-density polyethylene (HDPE). Our company has analyzed the subtle spectral differences using FT-IR. For more details, please refer to the PDF download below. 【Overview】 ■Polyethylene polymerization process ■IR measurement results ■Spectral overlay and spectral analysis ■Testing evaluation analysis services *For more information, please refer to the PDF document or feel free to contact us.

• Other contract services

Suitable for relative comparison of flat samples such as printed circuit boards! Introducing the analysis flow of liquid samples and solid surfaces.

We would like to introduce a case study of ion chromatography analysis conducted by our company (solid surfaces). Solid surfaces can also be measured using ion chromatography by extracting them into a solution. Additionally, average data can be obtained for sample surfaces larger than a few centimeters, making it suitable for relative comparisons of flat samples such as printed circuit boards. You can view the analysis flow for liquid samples and solid surfaces by downloading the PDF below. 【Overview of Liquid Sample Analysis】 ■ Liquid samples are introduced into the device for measurement after solution preparation such as dilution and filtration. ■ Measurement results are reported in solution concentration [mg/L]. *For more details, please refer to the PDF document or feel free to contact us.

• Other contract services

Identifying substances through various approaches such as insights, spectral analysis capabilities, and other analytical methods.

There are many types of thermoplastic resins, but among them, ABS is widely used in various products due to its unique molecular structure. As an engineering plastic, ABS resin is utilized in a wide range of fields, including electronic products, automobiles, home appliances, and IT-related products. We examined the characteristic IR spectrum of ABS resin using FT-IR analysis. [Shapes] ■Head to tail ■Head to head ■Tail to tail *For more details, please refer to the PDF document or feel free to contact us.

• Contract Analysis
• Other contract services

Analyze using information obtained from various analytical methods such as functional groups and skeletal structures! Introducing the mass spectrometry guide.

This document introduces a guide to mass spectrometry. In the analysis of organic compounds, information is obtained and analyzed from various analytical methods based on the functional groups, skeletal structures, and masses of the compounds. There are various methods for analyzing the mass of compounds, each with its own strengths in terms of the type of analysis and targets. Additionally, these methods can be selectively used according to the application or combined with other analytical techniques to obtain the necessary information. [Contents] ■ Methods mainly used in mass spectrometry - GC-MS - LC-MS - MALDI-TOFMS - GPC *For more details, please refer to the PDF document or feel free to contact us.

• Food Testing/Analysis/Measuring Equipment
• Analytical Equipment and Devices

It has been determined that the cause is due to cured ink adhering to the printed surface of the printed PET film!

We will introduce a case study on fish-eye analysis of laminated film. In the multi-layer laminated film used for containers such as refillable shampoos, a part resembling a foreign substance was observed. Upon magnified observation, it appeared to be several tens of micrometers in diameter and looked like a fish-eye. To clarify the cause, a cross-sectional observation was conducted. There are various methods for preparing cross-sections, but we implemented a mechanical polishing method that allows for extensive observation. [Case Overview] ■ Background: Discovered a part that appears to be a foreign substance in the multi-layer laminated film ■ Objective: Conducted cross-sectional observation to clarify the cause ■ Cross-section preparation method: Implemented a mechanical polishing method that allows for extensive observation *For more details, please refer to the PDF document or feel free to contact us.

• Surface treatment contract service
• Contract Analysis

Focusing on the position and composition of the foreign object! We prepared a cross-section of the foreign object and conducted elemental analysis.

We would like to introduce a case study of foreign matter analysis conducted on laminate film. Upon inspecting the back side of the laminate film, a black foreign object was identified. Therefore, we carried out an investigation to identify the layer of origin and component analysis of this black foreign object. First, we considered the methods based on the objectives of the analysis. This time, we focused on the position of the foreign object and its components, and decided to prepare a cross-section of the foreign object for elemental analysis. 【Case Overview】 ■ A black foreign object was identified upon inspecting the back side of the laminate film. ■ We conducted an investigation to identify the layer of origin and component analysis of the black foreign object. ■ We prepared a cross-section of the foreign object and conducted elemental analysis. *For more details, please refer to the PDF document or feel free to contact us.

• Surface treatment contract service
• Contract Analysis

Rich equipment and expertise! We will elucidate the molecular structures of materials in general through chemical instrument analysis!

There are various types of liquid crystal materials, including low molecular weight compounds used in LCD panels and high molecular weight polymers used in printed circuit boards and electronic components. We would like to introduce examples of molecular structure analysis of these low molecular weight liquid crystals and high molecular weight liquid crystals (LCP). Our company, equipped with a wealth of devices and expertise, can handle reliability testing and analytical analysis of not only liquid crystal materials but also various other materials. Please feel free to consult us regarding the understanding of molecular structures of imported overseas products and materials, as well as troubleshooting issues. 【Case Study Details】 ■ Molecular structure analysis using FT-IR ■ Understanding of surface functional groups (molecular groups) through XPS (ESCA) analysis ■ Example of LCD liquid crystal material analysis using GC-MS *For more details, please refer to the PDF document or feel free to contact us.

• Analytical Equipment and Devices
• Contract Analysis
• Contract Analysis

A reference peak was established in the ethylene section, focusing on the peaks involved in the ether bond!

This document introduces the analysis by Aites Inc. titled "Verification of Degree of Polymerization and Molecular Weight Differences through IR Analysis." Polyethylene oxide (PEO) is used in a wide range of applications due to its properties derived from its polar structure, including as an insulating material and electrolyte in lithium-ion polymer secondary batteries, surfactants, cosmetics, and synthetic detergent raw materials. In this study, we analyzed PEO with different degrees of polymerization and molecular weights using IR analysis, attempting to interpret the differences from the spectra and conduct data analysis. We invite you to read it. [Contents] ■ Polyethylene Oxide ■ Data analysis through overlaying IR spectra of each obtained sample ■ Other analytical methods are also possible *Please feel free to contact us.

• Analytical Equipment and Devices

Analysis of material structure and material properties, as well as discussions on defects and degradation phenomena using various analytical methods.

There are two main types of polyethylene resin: high-density polyethylene (HDPE) and low-density polyethylene (LDPE). While the basic molecular structure of each is the same, the differences in the number of branching structures and other factors result in different properties as polymers. Here, we present examples comparing HDPE and LDPE from various analyses. Our company not only analyzes material structures and properties but also examines variations in process conditions, defects, and degradation phenomena through various analytical methods. [Case Study Content] ■ Comparative analysis of main skeleton using FT-IR ■ Comparative analysis of thermal decomposition temperature using EGA-MS ■ Comparative analysis of thermal decomposition products using thermal decomposition GC-MS *For more details, please refer to the PDF document or feel free to contact us.

• Contract Analysis

The regulatory limit is 1000 ppm! You can easily check for the presence or absence of regulated compounds.

Phthalate esters are used as additive components, such as plasticizers, in many plastic products. However, under the revised RoHS directive, four new types of phthalate esters have become regulated substances. Our "screening analysis" allows for a simple examination of the presence or absence of regulated compounds. If a concentration of 500 to 1500 ppm is estimated, a more detailed quantitative analysis will be conducted for confirmation. In addition to the four types regulated by the RoHS directive, we can also perform a simple "screening analysis" for DNOP, DINP, and DIDP, which are regulated under JIG and the Food Sanitation Act. Please feel free to contact us for details about the samples and target compounds. 【Screening analysis of phthalate esters in bubble cushioning materials using Py-GC/MS】 ■Judgment criteria: Semi-quantitative values - Below 500 ppm: Determined as non-detect - Above 1,500 ppm: Determined as detect - 500 to 1,500 ppm: Re-examination will be conducted through quantitative analysis by solvent extraction *For more details, please refer to the PDF document or feel free to contact us.

• Contract Analysis

Confirmation methods for low molecular weight siloxanes! It is also possible to analyze the amount of occurrence.

It is known that low molecular siloxanes emitted from silicone products can cause the generation of silicon dioxide, an insulator, due to the heat of electrical sparks when present around the contacts of electronic components, leading to contact failures. Here, we introduce outgassing quantitative analysis using HS-GCMS as a method for confirming low molecular siloxanes. HS-GCMS analysis can determine whether there are materials around the electronic components that generate low molecular siloxanes and to what extent they are emitted. Please feel free to contact us regarding sample size and conditions. 【HS-GCMS Analysis of Silicone Adhesive Tapes】 - Tapes using silicone adhesives are sealed in a vial. - After heating at 130°C for 30 minutes, the emitted outgas is analyzed using headspace GCMS. - For the detected low molecular siloxanes, quantification was performed based on the equivalent of cyclic siloxane D5. *For more details, please refer to the PDF document or feel free to contact us.*

• Contract Analysis

For material evaluation and defect analysis! We will discuss the applied load and degradation mechanisms based on the differences in decomposition products.

Polycarbonate is a material that excels in impact resistance, weather resistance, and transparency, making it widely used in everything from industrial materials to everyday products. However, even polymers with excellent properties can undergo chemical changes, commonly referred to as degradation, due to the usage environment and the passage of time. This document presents examples of degradation analysis of polycarbonate materials subjected to UV irradiation and constant temperature and humidity testing. [Contents] ■ Thermal decomposition GC-MS analysis of polycarbonate *For more details, please refer to the PDF document or feel free to contact us.*

• Contract Analysis

It is possible to analyze with good sensitivity using thermal desorption GC-MS analysis! We propose methods tailored to the symptoms of issues and objectives.

Various additives are used in polymers to improve stability and processability; however, due to environmental impact and long-term storage, additive components may precipitate on the polymer surface, or the additives themselves may undergo chemical changes, leading to discoloration and degradation. This document presents examples of analyzing the bleed-out of additives and the chemical changes of additive components due to UV irradiation using thermal desorption GC-MS. Although additive components are present in only small amounts compared to the main polymer components, they can be analyzed sensitively using thermal desorption GC-MS. We propose methods tailored to specific issues or objectives, such as predicting product degradation in combination with reliability testing, thermal analysis, and main component analysis. Please feel free to contact us. [Contents] ■ Analysis of additive components bled out from nitrile rubber ■ Analysis of additive components in nylon 66 subjected to UV irradiation *For more details, please refer to the PDF document or feel free to contact us.

• Other analyses
• Contract Analysis
• Analysis Services

Measure the Raman spectrum! It is possible to obtain information about the structure and crystallinity of carbon materials.

Carbon materials include various types such as graphite, activated carbon, and carbon fibers, and are widely used in applications such as the active material for the negative electrode of lithium-ion batteries, additives for conductive plastics, inks, and CFRP. Our company evaluates the structural differences of carbon materials through Raman analysis. In the case of carbon black (CB) and activated carbon, the G-band peak becomes broader compared to graphite, and the full width at half maximum increases. This indicates that the crystallite size differs, with graphite having a larger crystallite size than CB and activated carbon. **Differences in Raman spectra due to carbon materials:** - Graphite shows a strong and sharp G-band around 1580 cm-1. - It indicates the disorder in the hexagonal structure, which is the unit cell of graphite, and the stacking of layers is more disordered. - In CB and activated carbon, the G-band peak is broader compared to graphite, and the full width at half maximum is larger. - Graphite has a larger crystallite size than CB and activated carbon. *For more details, please refer to the PDF document or feel free to contact us.*

• Analytical Equipment and Devices
• Contract Analysis

Wide-area image map driven by stage! Introducing a measurement example that visualizes the distribution of magic.

We will introduce a case of TOF-SIMS that enables wide-area image map measurement by combining it with an electric stage. We conducted wide-area (30mm × 30mm) image mapping measurements by drawing with two types of black markers on a metal plate. It is difficult to distinguish between the two types of markers in optical images, but by confirming the image map with characteristic secondary ion peaks for each marker, we can visualize the distribution of the markers. Additionally, there are cases where detailed analysis results were obtained from spectra after wide-area image map measurements using TOF-SIMS. [Overview] ■ Standard measurements (beam scan measurements) target sizes of 500μm × 500μm or smaller. ■ By combining with an electric stage, wide-area image map measurements are possible. *For more details, please refer to the PDF document or feel free to contact us.

• Contract measurement

Introducing the sample introduction device and the types of analytical samples and analysis content that each device specializes in!

GC-MS analysis is a method commonly used for the analysis of organic components and organic structure analysis. With auxiliary devices, it is capable of a wide range of analyses, from low molecular substances like solvents to high molecular substances like plastics. In this document, we will introduce the sample introduction devices owned by Aites, as well as the types of analysis samples and analysis content that each device specializes in. We invite you to read it. 【Contents】 ■ Overview ■ Conditions ■ Samples ■ Data Obtained ■ Analysis Examples *For more details, please refer to the PDF document or feel free to contact us.

• Analytical Equipment and Devices

Essential materials alongside metals and inorganic materials! Introducing examples of analysis and evaluation services for organic materials.

Organic materials such as solvents, additives, pharmaceuticals, and plastics are essential materials alongside metals and inorganic materials. They have a wide variety of types due to combinations of light elements, and their specificity arises from structures, intermolecular forces, and electron behavior. However, it seems that chemical instrumentation analysis and evaluation are necessary for a fundamental understanding of their properties. This document presents examples of analysis and evaluation services for organic materials. [Contents] ■ FT-IR analysis ■ GC-MS analysis ■ Molecular weight distribution evaluation by GPC (SEC) *For more details, please refer to the PDF document or feel free to contact us.

• Analytical Equipment and Devices

The analysis device also supports the analysis and evaluation of polymers! Information on the configuration and principles of high-temperature SEC equipment is provided!

The molecular weight of resins such as plastics is not a single value but is composed of multiple molecular weights. By understanding this molecular weight and its distribution, it leads to a better understanding of the characteristics and degradation mechanisms of the resin. In this document, we will introduce a case study where we measured polypropylene resin (PP) samples with and without ultraviolet (UV) irradiation using a high-temperature GPC device suitable for measuring polyolefin-based materials that are difficult to dissolve in solvents at room temperature, and conducted data analysis. We encourage you to read it. [Contents] ■ Configuration and principles of high-temperature SEC ■ Analysis case: Molecular weight measurement of PP subjected to UV irradiation ■ Application examples ■ Specifications and considerations for high-temperature SEC *For more details, please refer to the PDF document or feel free to contact us.

• Contract measurement
• Other analyses
• Contract Analysis

I will introduce examples of comparing the components of color developers contained in thermal paper using solvent extraction!

As a pre-treatment for GC-MS analysis, solvent extraction can sometimes allow for highly sensitive analysis of target substances. This document introduces examples of component comparison of dirt wiped with a cloth and component comparison of color developers contained in thermal paper using solvent extraction. In addition to solvent extraction, we can propose suitable methods from various pre-treatment techniques tailored to your samples and analysis targets, so please feel free to contact us. [Contents] ■ Comparative analysis of dirt components and surrounding materials ■ Component comparison of color developers contained in thermal paper *For more details, please refer to the PDF document or feel free to contact us.

• Contract Analysis
• Contract measurement
• Other contract services

Assist in the study of rocks and minerals! Raman spectroscopy is very effective for identifying and analyzing mineral species in rocks.

Introducing our Raman spectrum acquisition service for rocks. If you send us thinly sliced rock samples or extracted minerals and specify the measurement locations, we will obtain the Raman spectra for the specified locations. We also offer thin sectioning, elemental analysis (EDX/EPMA), and EBSD analysis. Please feel free to contact us when needed. 【Features】 ■ Raman spectra are very effective for identifying and analyzing mineral species in rocks. ■ If you send us thinly sliced rock samples or extracted minerals and specify the measurement locations, we will obtain the Raman spectra for the specified locations. ■ We also offer thin sectioning, elemental analysis (EDX/EPMA), and EBSD analysis. *For more details, please refer to the PDF document or feel free to contact us.

• Other contract services

Comparing thermal properties with DSC! We will discuss the impact of type identification and the state of polymer molecular chains on material properties!

Polyethylene (PE) comes in several types with different material properties depending on the length and number of its side chain branches. From the melting peak of crystalline polyethylene, the melting point and crystallinity were measured using DSC and compared for each type of polyethylene. LDPE, which has many long side chains and is less dense, resulted in a low melting point and low crystallinity, while HDPE, which tends to have a denser molecular chain, showed high values for both melting point and crystallinity. Additionally, LLDPE, which has many relatively short side chains and is easier to densify than LDPE, exhibited intermediate values for melting point and crystallinity between LDPE and HDPE. [Types of Polyethylene] - LDPE (Low-Density Polyethylene): Low rigidity and high flexibility - LLDPE (Linear Low-Density Polyethylene): Tougher than LDPE but less processable - HDPE (High-Density Polyethylene): High rigidity, excellent tensile strength, impact strength, and hardness *For more details, please refer to the PDF document or feel free to contact us.

• Analytical Equipment and Devices
• Contract measurement
• Other contract services

GC-MS is used for qualitative and quantitative analysis of low molecular organic substances! Data was obtained and compared using incense and sandalwood!

Using fragrance as a keyword, we analyzed common incense and compared the characteristics of its molecular structure with other materials. The three representative fragrant woods obtained from trees are sandalwood, agarwood, and kyara, but this time we collected data on incense and sandalwood. With aldehyde groups and aliphatic cyclic structures as features, it is speculated that the woody scent is mainly due to the aliphatic cyclic structure. [Analysis Overview] ■ Analysis Samples: Incense, Sandalwood ■ Identification of fragrance components by thermal desorption GC-MS (180°C) - Confirmed peaks with the same detection time as sandalwood - Indicates that sandalwood is used as a fragrance in the incense *For more details, please refer to the PDF document or feel free to contact us.

• Analytical Equipment and Devices
• Contract Analysis
• Other contract services

The aldol reaction progresses under the influence of temperature, humidity, and light! Example of impurity analysis in ethanol and acetone.

This is an example of analyzing impurities confirmed from a solvent when high-purity products are stored in inappropriate environments, using liquid injection GC-MS. Ethanol stored in a light-protective reagent bottle in a cool, dark place was transferred to a used plastic wash bottle and left at room temperature for about a month. As a result, impurities such as triethyl borate and alkylbenzenes were detected. Additionally, acetone stored in a light-protective reagent bottle in a cool, dark place was transferred to a transparent glass bottle without light protection and left at room temperature for about a month, resulting in the detection of diacetone alcohol as an impurity. [Impurity Analysis in Ethanol] ■ Ethanol stored in a light-protective reagent bottle in a cool, dark place was transferred to a used plastic wash bottle and left at room temperature for about a month (the opening of the wash bottle was not sealed). ■ Result: Impurities such as triethyl borate and alkylbenzenes were detected. *For more details, please refer to the PDF document or feel free to contact us.

• Analytical Equipment and Devices
• Contract Analysis
• Other contract services

Depending on the panel size, it is possible to analyze using different ICP-AES/MS devices!

We will introduce a case where ICP measurement was conducted using panels before and after reliability testing, along with quantification. The liquid crystal molecules in an LCD are oriented within the panel, and the display is controlled by changes in the orientation state of the liquid crystal due to voltage. When ionic substances, such as metal elements, are present inside the panel, the liquid crystal does not operate correctly, leading to display defects. Ionic substances are known to increase due to contamination during manufacturing or long-term use, making it important to quantify and understand them as part of panel quality. Metal ions can be quantitatively analyzed using ICP analysis, and depending on the differences in pretreatment methods and detection sensitivity, ICP-AES and ICP-MS are used selectively. [Analysis Content] ■ Comparison of metal element content using ICP-AES analysis ■ Comparison of metal element content using ICP-MS analysis *For more details, please refer to the PDF document or feel free to contact us.

• Analysis Services

Focusing on sandalwood (Byakudan), which is used as a raw material for incense! Here is an example of component analysis using GC-MS.

Due to the risk of depletion of natural ingredients, artificially synthesized alternative components may be used, and their identification is suitable for separation and analysis using methods such as GCMS. This time, we focused on sandalwood (Byakudan), which is used as a raw material for incense. We tested whether the components of sandalwood could be detected in two types of incense (A and B) with its fragrance. In incense A, santanol was detected, while in incense B, santanol was not detected, and another fragrant component was found. Among these, bugdanol is a type of synthetic fragrance, and due to its structural characteristics, it is believed to have a sandalwood-like scent. [Components of Incense A] ■ Bugdanol: Trace amounts ■ Cedrol: None ■ α-Santalol: Present ■ β-Santalol: Present *For more details, please refer to the PDF document or feel free to contact us.

• Analytical Equipment and Devices
• Contract Analysis

We assist in manufacturing and research and development with a focus on SDGs by conducting comparative analysis and evaluation of recycled materials and raw materials using multiple methods.

A commitment to environmental consideration and waste-free development and manufacturing is required in the field of technology, and there is a need for global contributions to technology from a planetary perspective. This document introduces case studies that identify the substances of discarded and floating microplastics and compare the degradation levels of recycled materials, assisting in the determination of their usability. Please take a moment to read it. [Contents] ■ Case studies on the identification and analysis of microplastic substances ■ Comparative analysis of molecular weight distribution between unused polypropylene materials and recycled products (pellets) ■ Comparative analysis of polyethylene terephthalate (PET) materials using microscopic IR analysis *For more details, please download the PDF or feel free to contact us.

• Water quality testing

Spectroscopic analysis is suitable for component analysis and qualitative analysis of foreign substances.

We will introduce the comparison between Raman spectroscopy analysis by Aites Co., Ltd. and FTIR. Spectroscopic analysis is suitable for component analysis of foreign substances and qualitative analysis. Both Raman and FT-IR can obtain spectra based on the structure of the analysis target. However, since each has its strengths and weaknesses, it is necessary to choose between the two depending on the analysis target. 【Features】 ■ Measurement in the order of several micrometers, which is difficult to analyze with IR, is possible. ■ No sampling is required. *For more details, please refer to the PDF materials or feel free to contact us.

• Testing Equipment and Devices

The purity of the electrolyte greatly affects the performance of the battery! It suppresses the volatility of sulfur components and converts them into a form that can be detected by IC.

We would like to introduce an example of analyzing the purity of phosphorus pentasulfide using ion chromatography for the composition analysis of raw materials for all-solid-state batteries. Phosphorus pentasulfide is one of the raw materials used in the production of electrolytes for sulfide-based all-solid-state batteries. As a pretreatment for IC measurement, the powder of phosphorus pentasulfide was dissolved in alkaline water and converted into phosphate and sulfide salts. Subsequently, sulfide ions were oxidized to sulfate ions to prepare the IC measurement solution. For more details, please refer to the published catalog. 【Solid Electrolytes (Partial)】 ■Li3PS4 ■Li7P3S11 ■Li6PS5Cl ■Li6PS5Br *For more information, please refer to the PDF materials or feel free to contact us.

• Analytical Equipment and Devices

By conducting two analyses, it is possible to obtain more detailed and accurate results!

This document introduces the characteristics of each spectroscopy method and the spectra obtained when comparing infrared spectroscopy and Raman spectroscopy. Both infrared spectroscopy and Raman spectroscopy are vibrational spectroscopies that investigate the vibrational energy of molecules, but the shapes of the spectra obtained from each method differ even when measuring the same substance. Infrared spectroscopy and Raman spectroscopy are complementary; information that cannot be obtained through a single analysis can be acquired more detailed and accurately by conducting both analyses. For more details, please refer to the catalog provided. 【Characteristics of Infrared Spectroscopy】 ■ Infrared absorption occurs when the dipole moment changes with vibration (infrared active). ■ Vibrations that cause a distortion in the symmetry of the molecule (leading to an electronic dipole) are highly infrared active. *For more information, please refer to the PDF materials or feel free to contact us.

• Vibration Testing

It is possible to investigate components that cannot be identified by spectroscopy alone, as well as trace additives that cannot be detected!

This is an introduction to the analysis of the components of mica sheet adhesives using GC/MS. To investigate what components are contained in the mica sheet, spectroscopic measurements were conducted, suggesting that silicone-based adhesives are used. To examine the composition of the silicone-based adhesive, GC/MS measurements were performed. It was found that pentacyclooctasiloxane is used, and it was also discovered that dibutyl phthalate is added as a plasticizer and chain-saturated hydrocarbons such as tridecane are added as lubricants. 【Components of the mica sheet】 ■ Pentacyclooctasiloxane (cage-like polymethylsilsesquioxane) ■ Dibutyl phthalate ■ Chain-saturated hydrocarbons such as tridecane *For more details, please refer to the PDF document or feel free to contact us.

• Analytical Equipment and Devices
• Spectroscopic Analysis Equipment

Proposals tailored to the purpose of analysis and the target object! GC/MS analysis of derivatized samples.

This document introduces a pretreatment method to enable the analysis of substances that are difficult to analyze using GC/MS. The pretreatment that converts difficult-to-analyze substances into analyzable substances is called "derivatization." Methods such as esterification, acylation, and silylation are used selectively according to the type and characteristics of the difficult-to-analyze substances. GC/MS measurements were conducted on citric acid solutions and citric acid solutions after esterification. It was found that citric acid, being a carboxylic acid, could not be effectively detected without derivatization, but after esterification, trimethyl citrate was detected, confirming the presence of citric acid. By performing appropriate derivatization, more accurate analysis becomes possible. [Analyzable Substances] ■ High volatility ■ High thermal stability ■ Low polarity *For more details, please refer to the PDF document or feel free to contact us.

• Analytical Equipment and Devices

Important analysis items for performance evaluation and quality control of functional materials! Evaluation of pore size and pore distribution of non-woven sheets and membrane materials.

This is an example of evaluating the maximum pore diameter and pore size distribution of non-woven fabric sheets using the bubble point method. The sample is immersed in a chemical solution and air pressure is applied. The pressure is increased until it overcomes the surface tension of the chemical solution absorbed in the sheet, resulting in the appearance of bubbles; this pressure is referred to as the bubble point. The maximum pore diameter can be calculated based on the bubble point pressure and the surface tension of the chemical solution. 【Calculation Formula】 ■d = Cy/P ・d: Maximum pore diameter ・C: Constant ・y: Surface tension of the chemical solution ・P: Differential pressure *For more details, please refer to the PDF document or feel free to contact us.

• Analytical Equipment and Devices

The Raman spectrum reflects the functional groups of organic compounds! The curing reaction can be estimated to some extent.

Our company analyzes the spectra of UV-curable resins before and after UV irradiation. We irradiate UV-curable resin (acrylic type) with ultraviolet light and obtain Raman spectra before and after irradiation. Through the analysis of the Raman spectra, the curing reaction can be estimated to some extent. For a more detailed analysis of the curing mode, analyses such as GCMS are necessary, but our company can provide not only structural estimation but also reaction estimation through spectral analysis. 【Features of Raman Spectral Analysis】 ■ The curing reaction can be estimated to some extent. ■ We provide support for both structural estimation and reaction estimation. *For more details, please refer to the PDF materials or feel free to contact us.

• plastic
• Contract Analysis

The "Mechanical Stitching Method" by Nichinichisui Road Machinery Co., Ltd. is a new technique that allows for the repair of metal cracks without the application of heat. By using special bolts and reinforcement plates, cracks are physically removed, and repairs are made without causing any thermal impact on the base material. Repairs can be carried out even in environments where open flames cannot be used. Since no heat is applied, the disassembly of equipment is kept to a minimum. ◎ For more details, please contact us. ◎ If a detailed technical explanation is needed, please contact us.

The "Mechanical Stitching Method" by Nichinichisui Road Machinery Co., Ltd. is a new technique that allows for the repair of metal cracks without the application of heat. By using special bolts and reinforcement plates, cracks are physically removed, and repairs are made without any thermal impact on the base material. Repairs can be conducted in environments where open flames cannot be used. Since no heat is applied, the disassembly of equipment is minimized. ◎ For more details, please contact us. ◎ If a detailed technical explanation is required, please contact us.

When measuring the flow rate of liquids or gases that are unsuitable for plastic due to high pressure or high temperature, our robust "glass tube variable area flow meter (rotameter)" allows for more accurate flow measurements. It offers a wider flow range and is suitable for various liquids and gases! 【Features】 ■ Glass tube variable area flow meter ・ Flow measurement technology with high durability, economy, and excellent operability ・ Capable of a wider flow range, suitable for various liquids and gases ■ Metal tube variable area flow meter ・ Durability and accuracy that withstands high pressure and harsh temperature environments 【Product Lineup】 ■ Glass tube variable area flow meter ・ Sho-Rate models 1350, 1355, 1358 ・ GT1600 series ■ Metal tube variable area flow meter ・ MT3750 series ・ MT3809 series ▼ For more details, visit https://www.brooksinstrument.com/ja-jp/products/variable-area-flow-meters

The "Mechanical Stitching Method" by Nichinichisui Road Machinery Co., Ltd. is a new technique that allows for the repair of metal cracks without the application of heat. By using special bolts and reinforcement plates, cracks are physically removed, and repairs are made without affecting the base material with heat. Repairs can be carried out in environments where open flames cannot be used. Since no heat is applied, the disassembly of equipment is minimized. ◎ For more details, please contact us. ◎ If a detailed technical explanation is needed, please contact us.

The "Mechanical Stitching Method" by Nichinichisui Road Machinery Co., Ltd. is a new technique that allows for the repair of metal cracks without the application of heat. By using special bolts and reinforcement plates, cracks are physically removed, and repairs are made without causing any thermal impact on the base material. Repairs can be carried out even in environments where open flames cannot be used. Since no heat is applied, the disassembly of equipment is minimized. ◎ For more details, please contact us. ◎ If a detailed technical explanation is needed, please contact us.