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  3. 一般財団法人材料科学技術振興財団 MST
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一般財団法人材料科学技術振興財団 MST

EstablishmentAugust 1, 1984
addressTokyo/Setagaya-ku/Kitaomi 1-18-6
phone03-3749-2525
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last updated:May 26, 2025
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一般財団法人材料科学技術振興財団 MST List of Products and Services

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Mass spectrometry Mass spectrometry
 【分析事例】高分子材料 【分析事例】高分子材料
【測定法】計算科学・AI・データ解析 【測定法】計算科学・AI・データ解析
Photoelectron spectroscopy Photoelectron spectroscopy
[Measurement Method] Electron Microscopy Observation and Analysis [Measurement Method] Electron Microscopy Observation and Analysis
Vibrational spectroscopy Vibrational spectroscopy
Measurement Method: X-ray Diffraction Related Measurement Method: X-ray Diffraction Related
[Measurement Method] Related to SPM [Measurement Method] Related to SPM
Measurement Method: Failure Analysis Measurement Method: Failure Analysis
[Measurement Method] Other Measurement Methods [Measurement Method] Other Measurement Methods
Processing methods and treatment methods Processing methods and treatment methods
Other services and support information Other services and support information
[Analysis Case] LSI・Memory [Analysis Case] LSI・Memory
[Analysis Case] Optical Devices [Analysis Case] Optical Devices
[Analysis Case] Solar Cells [Analysis Case] Solar Cells
[Analysis Case] Fuel Cell [Analysis Case] Fuel Cell
[Analysis Case] Display [Analysis Case] Display
[Analysis Case] Oxide Semiconductors [Analysis Case] Oxide Semiconductors
[Analysis Case] Power Device [Analysis Case] Power Device
[Analysis Case] Electronic Components [Analysis Case] Electronic Components
[Analysis Case] Secondary Battery [Analysis Case] Secondary Battery
[Analysis Case] Lighting [Analysis Case] Lighting
[Analysis Case] Manufacturing Equipment and Components [Analysis Case] Manufacturing Equipment and Components
[Analysis Case] Biotechnology [Analysis Case] Biotechnology
[Analysis Case] Cosmetics [Analysis Case] Cosmetics
[Analysis Case] Food [Analysis Case] Food
[Analysis Case] Pharmaceuticals [Analysis Case] Pharmaceuticals
[Analysis Case] Medical Devices [Analysis Case] Medical Devices
Analysis Case: Daily Necessities Analysis Case: Daily Necessities
[Analysis Case] Environment [Analysis Case] Environment
[Analysis Case] Others [Analysis Case] Others
Materials from the exhibition where MST exhibited. Materials from the exhibition where MST exhibited.
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[Analysis Case] Evaluation of Surface Components of Fur

It is possible to quantify the surface condition through surface analysis of animal fur (coat)!

The surface of human hair (hair) is covered with a lipid called 18-methyl eicosanoic acid (18-MEA). The surface of animal fur (coat) is believed to contain various lipids secreted from sebaceous glands, not limited to 18-MEA. Additionally, a decrease in linoleic acid has been reported in the sebum of animals with skin diseases. Therefore, simultaneously analyzing the representative lipid 18-MEA along with several other components is useful for understanding the condition of the hair. This document presents the results of evaluating the differences in lipids for each type of animal (pet) using TOF-SIMS.

  • Contract measurement
  • Time-of-flight mass spectrometer
  • Contract Inspection

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[Analysis Case] Contamination Analysis in Vacuum Equipment

It is possible to evaluate the causes of contamination in vacuum devices, such as oil backs and grease!

Vacuum devices that utilize the characteristic of low gas molecular density in a space are used in various applications such as thin film formation and surface analysis in the manufacturing process of electronic components. Since the chamber of a vacuum device is a closed space, the presence of trace amounts of molecules can easily cause contamination within the device. To suppress contamination, it is necessary to conduct investigations to identify contamination sources such as pumps, devices, and samples. This document presents a case study investigating contamination within a vacuum device using TOF-SIMS.

  • Contract measurement
  • Surface treatment contract service
  • Time-of-flight mass spectrometer

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[Analysis Case] Investigation of Foreign Object Occurrence: Analysis of the Tube

It is possible to estimate the cause of wafer contamination!

TOF-SIMS is a very effective method for investigating the causes of contamination due to foreign substances, deposits, dirt, discoloration, and other factors related to the process. By comparing the mass spectral information obtained from contamination such as foreign substances with the mass spectral information of candidate contamination source components, it is possible to infer the sources of that contamination. In this document, we prepared four types of resin tubes used in the wafer manufacturing process and foreign substances on Si wafers, and by comparing their mass spectral information, we evaluated which components used in the process the contamination from the foreign substances was attributed to.

  • Contract measurement
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  • Time-of-flight mass spectrometer

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[Analysis Case] Internal Structure Evaluation of Battery Components Using Nano-CT

Observe the fine structure inside the sample in three dimensions with a spatial resolution of 100 nm!

Nano-CT is a type of X-ray CT that uses synchrotron radiation as a source and allows for three-dimensional observation of the internal structure of samples with a spatial resolution of about 100 nm. This document presents a case study that visualizes the internal structure of battery components sealed in laminate film. Through nano-CT measurements, it is possible to confirm the fine structures and cracks of active materials that could not be captured by conventional micro-CT (spatial resolution of 1 μm or more).

  • Contract measurement
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  • X-ray inspection equipment

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[Analysis Case] Vapor Pressure Calculation of Ga-containing Precursor by Molecular Dynamics Simulation

Effective for predicting the vapor pressure of metal complexes used as precursors in ALD and CVD!

ALD (Atomic Layer Deposition) is a method that allows for uniform film formation at the atomic layer level, even for high aspect ratio structures, and is being focused on as a useful technique for the miniaturization, integration, and fine wiring of semiconductors. Since it is a vapor-phase deposition method that utilizes the "adsorption saturation of precursors on the growth surface," high vapor pressure precursors are required to improve the coverage rate of precursors on the substrate and the deposition rate. This document predicts the vapor pressures of various Ga-containing precursors through molecular dynamics calculations and compares them with experimental values.

  • Contract Analysis
  • Computational Chemistry
  • simulator

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[Analysis Case] Evaluation of Bacterial Count by Real-Time PCR Method

We will analyze the bacteria in the sample from DNA without isolation or cultivation!

The measurement of bacterial counts conducted in food bacterial testing is calculated by culturing and counting the number of colonies. However, this method requires time for culturing and cannot evaluate difficult-to-culture bacteria. On the other hand, the real-time PCR method allows for the direct extraction of DNA from samples without culturing, enabling the investigation of the quantity of the target bacteria (DNA copy number). This document presents a case study comparing the bacterial counts obtained through culturing the easily cultured Escherichia coli and the copy numbers measured using the real-time PCR method.

  • Contract measurement
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  • Real-time PCR

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[Analysis Case] Depth Direction State Evaluation of Tin (Sn) Surface

Evaluation of modified layers and altered layers through surface treatment is possible!

TOF-SIMS has good depth resolution and can obtain fragment ions corresponding to bonding states, allowing for the evaluation of layer structures near the surface, within a few nanometers. This document presents a case study analyzing the layer structure of a tin plate surface based on the information obtained from the measurement of standard samples of tin oxide and hydrated tin oxide. By applying this technology, it is possible to evaluate modified layers and altered layers due to surface treatment.

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[Analysis Case] CO2 Adsorption Simulation on MOF using GCMC Method

The adsorption properties of nano-porous materials such as MOF and zeolite can be predicted!

MOFs (Metal-Organic Frameworks) are attracting attention as nano-porous materials with potential applications in separation processes, catalysis, and gas storage. The combinations of MOF topology, linkers, and metal nodes are vast, and the types of synthesizable MOFs are virtually limitless. Therefore, prior screening and understanding of the structure, function, and properties are crucial for the development of new MOF materials. In this case study, we predicted the CO2 adsorption amounts for various MOFs using the GCMC (Grand Canonical Monte Carlo) method and examined the factors affecting the adsorption characteristics.

  • Contract Analysis
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  • simulator

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[Analysis Case] Diamond Evaluation Case Using SIMS

It is possible to quantitatively evaluate impurity elements and assess film thickness.

Diamonds possess excellent physical properties such as high breakdown electric fields, making them promising materials for next-generation power devices and quantum devices. By doping diamonds with impurity elements, they can function as high-performance semiconductors. To understand the concentration distribution of the doped elements, SIMS analysis, which can detect impurities in the ppb to ppm range with high sensitivity, is effective. Additionally, it is possible to evaluate the film thickness of each layer from the impurity concentration distribution. MST offers a variety of diamond standard samples and can quantify over 30 different elements.

  • Contract measurement
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  • Mass Spectrometer

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[Analysis Case] HF Etching Simulation of a-SiO2 Film

Effective for understanding surface reactions at the atomic level in the etching process.

With the miniaturization of semiconductor processes, the importance of surface reactions due to etching gases, precursors in ALD film formation, and plasma treatments is increasing. For systems involving complex chemical reactions such as etching, changes in surface bonding states, and defect generation, analysis using molecular dynamics calculations is effective for understanding phenomena at the atomic level. This document evaluates the HF etching reaction of a-SiO2 using molecular dynamics calculations. A similar approach can be applied to various reactions and materials.

  • Contract measurement
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  • simulator

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[Presentation] Surface analysis applicable in various fields! TOF-SIMS Analysis Case Studies

From inorganic to organic materials, leave high-sensitivity surface analysis to us!

TOF-SIMS analysis allows for detailed examination of the sample's outermost surface, as well as the ability to obtain information in the depth direction, making it possible to understand the distribution of components within the material. Additionally, imaging can visualize the spatial distribution of components. This document includes case studies of products analyzed from various fields. Please feel free to contact us!

  • Contract measurement
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Analysis Case: Analysis of Defect Levels in Gallium Nitride

You can obtain various physical property information such as point defect formation energy, charge, and optical transitions!

Our organization conducts an analysis of defect levels in wide bandgap semiconductor gallium nitride (GaN) using first-principles calculations. Gallium nitride (GaN), a wide bandgap semiconductor, is primarily used in the field of power devices, and in recent years, there has been an increasing demand for applications such as rapid chargers and 5G communication base stations. Here, we present a case study analyzing the defect levels formed by nitrogen vacancies (VN) in GaN using first-principles calculations. [Measurement and Processing Methods] ■ [PL] Photoluminescence Method ■ Computational Science, AI, Data Analysis *For more details, please download the PDF or feel free to contact us.

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[Analysis Case] Investigation of Product Deterioration through Weather Resistance Testing

It is possible to reproduce the deterioration state using the Sunshine Weather Meter!

Our organization conducts product degradation investigations through weather resistance testing. The Sunshine Weather Meter can artificially reproduce sunlight, temperature, humidity, and other conditions. We conducted weather resistance testing standards for bicycle lights and examined changes over time. To quantitatively discuss the discoloration of lights that are originally black, we refer to (JIS D 0205) and present a case study evaluating color difference and glossiness. 【Measurement Methods and Processing Methods】 ■Others ■Weather Resistance Testing *For more details, please download the PDF or feel free to contact us.

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Analysis case: Assignment of the Raman spectrum of copper phthalocyanine.

By combining actual measurements and simulations, detailed peak attribution is possible!

Our organization is conducting the assignment of the Raman spectrum of copper phthalocyanine through quantum chemical calculations. By comparing the measured results with the simulation results from quantum chemical calculations, we can perform spectral assignment, which allows for the analysis of vibrational modes. Here, we will introduce a case study of the analysis of "copper phthalocyanine," which is also expected to be utilized in organic thin-film transistors and other applications. 【Measurement and Processing Methods】 ■ [Raman] Raman Spectroscopy ■ Computational Science, AI, Data Analysis *For more details, please download the PDF or feel free to contact us.

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[Analysis Case] Imaging of Lipids

Imaging of lipids in mouse testis! Introducing cases measured with TOF-SIMS and MALDI-MS.

Our organization conducts lipid imaging. TOF-SIMS excels in low-mass components and enables imaging with high spatial resolution. On the other hand, MALDI-MS specializes in high-mass components and offers a wide variety of lipids that can be imaged. Here, we present examples of measurements taken with TOF-SIMS and MALDI-MS, using lipid imaging mass spectrometry results from mouse testes as a case study. [Measurement Methods] ■ [TOF-SIMS] Time-of-Flight Secondary Ion Mass Spectrometry ■ [MALDI-MS] Matrix-Assisted Laser Desorption Ionization Mass Spectrometry *For more details, please download the PDF or feel free to contact us.

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[Analysis Case] Evaluation of Hierarchical Structure of Polymer Materials Using X-ray Diffraction and Scattering Techniques

Structural analysis of lamellae and similar structures is possible! Similar evaluations can be performed using WAXS (Wide-Angle X-ray Scattering).

Our organization conducts evaluations of the hierarchical structure of polymer materials using X-ray diffraction and scattering techniques. It is known that the differences in higher-order structures created by amphiphilic substances affect the moisturizing and permeability properties of skin tissue, making it important to understand these structures in order to evaluate the functionality of the materials. We will introduce examples of evaluating the hierarchical structure of polymers using XRD (X-ray diffraction) for structures on the order of a few nanometers and SAXS (small-angle X-ray scattering) for structures on the order of several tens of nanometers. 【Measurement and Processing Methods】 ■ [XRD] X-ray Diffraction ■ [SAXS] Small-Angle X-ray Scattering *For more details, please download the PDF or feel free to contact us.

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[Analysis Case] Calculation of Acid Dissociation Constant (pKa) Using Quantum Chemistry Calculations

It is possible to predict the pKa of compounds with unknown pKa based on calibration curves created for each solvent and functional group!

Our organization conducts calculations of acid dissociation constants (pKa) using quantum chemistry. The acid dissociation constant (pKa) is one of the indicators that quantitatively represents the strength of an acid (the ease of proton dissociation). Knowing the pKa helps in estimating the solubility of compounds in relation to pH, their state, the ease of absorption of pharmaceuticals in the body, and pH buffering effects. Using the acid dissociation energy differences obtained from quantum chemical calculations and experimental pKa values, we create calibration curves for different solvents and functional groups, and present examples of studies investigating the impact of intramolecular hydrogen bonding on pKa. [Measurement Methods and Processing Methods] ■ Computational Science, AI, Data Analysis *For more details, please download the PDF or feel free to contact us.

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[Analysis Case] Evaluation of Molecular Permeability to Lipid Bilayers through Molecular Dynamics Calculations

Insights into the permeability of molecules can be obtained from free energy calculations!

Our organization conducts evaluations of molecular permeability to lipid bilayers using molecular dynamics simulations. The free energy obtained from molecular dynamics calculations is an important value that contributes not only to predicting the stability of the system but also to understanding the material distribution and transport phenomena in systems with spatial and temporal fluctuations. For example, it is effective in gaining insights into the permeability of molecules across biological membranes. Using lipid bilayers in aqueous solvents as an example, we will introduce a case where the permeability of molecules in the membrane was discussed based on the free energy values when benzene and carbon dioxide were transported. [Measurement Methods and Processing Techniques] ■ Computational Science, AI, Data Analysis *For more details, please download the PDF or feel free to contact us.

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[Analysis Case] Analysis of Thermal Decomposition Reactions of Ionic Liquids through Quantum Chemical Calculations

Reactivity can be evaluated from the activation energy values obtained from the simulation!

Our organization conducts analyses of the thermal decomposition reactions of ionic liquids using quantum chemical calculations. Since ionic liquids are often used at high temperatures for extended periods, understanding their reactivity, such as thermal decomposition, is essential. We will introduce examples of evaluating the likelihood of thermal decomposition reactions of ionic liquids through quantum chemical calculations. 【Measurement Methods and Processing Methods】 ■Computational Science, AI, Data Analysis *For more details, please download the PDF or feel free to contact us.

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[Analysis Case] Evaluation of Binding States in Secondary Battery Cathodes

You can evaluate the sample in its original state, from the binder and coating to the active substance.

Our organization conducts evaluations of the bonding state of cathodes in secondary batteries. X-ray photoelectron spectroscopy (XPS), which is one of the methods for analyzing surface states, is suitable for evaluating binders and conductive additives due to its shallow detection depth (approximately 10 nm). Hard X-ray photoelectron spectroscopy (HAXPES), which uses hard X-rays (Ga rays) for excitation, allows us to obtain information about active materials buried under binders without causing damage, thanks to its deeper detection depth. 【Measurement and Processing Methods】 ■ [XPS] X-ray Photoelectron Spectroscopy ■ [HAXPES] Hard X-ray Photoelectron Spectroscopy ■ Processing under controlled atmosphere *For more details, please download the PDF or feel free to contact us.

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[Analysis Case] Metal Analysis in Organic Materials

Microwave decomposition combined with ICP-MS! Metal analysis in organic materials is possible.

Our organization conducts metal analysis in organic materials. Metal components can cause a decrease in insulation properties when they contaminate organic materials, such as in semiconductor devices. Therefore, it is important to understand the amount of metal in organic materials. In this case, we analyzed the metal content in organic materials (polyethylene products, polypropylene products, polyimide films). Organic materials can be acid-digested by irradiating them with microwaves in a sealed state (under high temperature and pressure). [Measurement Method / Processing Method] ■ [ICP-MS] Inductively Coupled Plasma Mass Spectrometry *For more details, please download the PDF or feel free to contact us.

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[Analysis Case] Observation of Structural Changes in ABS Resin through Tensile Testing

Monitor three-dimensional structural changes! It is possible to observe the three-dimensional structure under load applied to the sample.

Our organization conducts observations of structural changes in ABS resin through tensile testing using in situ X-ray CT. In in situ X-ray CT measurements, it is possible to perform structural observations while applying a load (tensile or compressive) to the sample. In this case, X-ray CT measurements were conducted on a sample of ABS resin containing glass filler under tensile load, and the tensile stress applied to the sample was calculated. The three-dimensional structural changes of the resin and glass filler under each stress condition were monitored. [Measurement Method / Processing Method] ■ X-ray CT Method *For more details, please download the PDF or feel free to contact us.

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[Analysis Case] Energy Profile of Li Ion Insertion/Extraction Process

Information on the energy barrier during Li-ion de-insertion and the solvent formation process can be obtained!

Our organization provides the energy profile of the Li-ion insertion and extraction process in LIB anodes/electrolytes using the ESM-RISM method. During the charge and discharge processes of lithium-ion secondary batteries (LIB), various phenomena occur near the interface with the electrolyte and the anode, including the formation of solvation, desolvation, the formation of the electric double layer, and the insertion and extraction of Li ions. This document introduces a case study that evaluates the energy profile and solvation structure during the Li-ion insertion and extraction process from graphite anodes using the hybrid ESM-RISM method, which combines Effective Screening Medium (ESM) and Reference Interaction Site Model (RISM) through simulation. [Measurement and Processing Methods] ■ Computational Science, AI, Data Analysis *For more details, please download the PDF or feel free to contact us.

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[Analysis Case] Structural Analysis of End Groups of Polycarbonate

End groups of polycarbonate can be distinguished by the manufacturing method using thermal decomposition GC/MS!

Our organization offers analysis of the end group structure of polycarbonate. Polycarbonate is an engineering plastic known for its excellent impact resistance and heat resistance, and it is widely used as a material in electrical, electronic, and optical devices. There are mainly two methods of manufacturing polycarbonate, and the end group structure, which affects the physical properties of the polymer, varies depending on the manufacturing method. Since the end group portion of the polymer is small compared to the main chain, the analytical methods available for its structural analysis are limited. Here, we present a case study evaluating the end group structure of polycarbonate using thermal decomposition GC/MS. [Measurement Method / Processing Method] ■ [GC/MS] Gas Chromatography Mass Spectrometry *For more details, please download the PDF or feel free to contact us.

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[Analysis Case] NMR Chemical Shift Simulation of Organic Molecules

It is possible to identify structural isomers through analysis that combines measurement and calculation!

Our organization conducts NMR chemical shift simulations of organic molecules using quantum chemical calculations. Determining the isomeric structures of organic molecules is a very important issue in fields such as natural product chemistry and drug discovery. Combining the results of nuclear magnetic resonance (NMR) measurements with NMR chemical shift simulation results from quantum chemical calculations is believed to be useful for elucidating the structures and evaluating the properties of novel compounds that lack model compounds for structure-chemical shift correlation. This document presents a case study on the identification of structural isomers of biologically active quinoxaline derivatives. [Measurement Methods and Processing Methods] ■ [NMR] Nuclear Magnetic Resonance Analysis ■ Computational Science, AI, Data Analysis ■ Others *For more details, please download the PDF or feel free to contact us.

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[Analysis Case] Oil Analysis (GC/MS Edition)

When oil contamination is suspected, it is possible to distinguish between types of oil and estimate the source!

Our organization is capable of identifying the composition of petroleum products, evaluating molecular weight distribution, and distinguishing types of oils. Petroleum products such as oils and greases are mixtures of hydrocarbons with various compositions, and GC/MS methods are effective for their qualitative analysis. Here, we present a case study where commercially available oils with different molecular weight distributions were measured using soft ionization methods. Compared to hard ionization methods (EI), soft ionization methods (FI and FD) allow for the detection of molecular ions, making them effective for evaluating the composition of oil components. In particular, the FD method can also be applied to evaluate oils containing high molecular weight components that are difficult to volatilize. [Measurement Method / Processing Method] ■ [GC/MS] Gas Chromatography Mass Spectrometry *For more details, please download the PDF or feel free to contact us.

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[Analysis Case] Fine Structure of Hair Cross-Section (S)TEM Analysis

We will introduce examples of observations of hair cell membrane complexes (CMC)!

Our organization offers (S)TEM analysis of the fine structure of hair cross-sections. The hair cell membrane complex (CMC) serves as a pathway for chemicals during processes such as bleaching and dyeing hair. In particular, the CMC between the cuticle layers has a three-layer structure, which we have visualized. We present a case where osmium tetroxide (OsO4) was used for electron staining targeting unsaturated fatty acids in lipids, followed by TEM observation and STEM-EDX analysis. [Measurement and Processing Methods] ■ [(S)TEM] Scanning Transmission Electron Microscopy ■ [TEM-EDX] Energy Dispersive X-ray Spectroscopy (TEM) ■ Ultramicrotome processing ■ Others *For more details, please download the PDF or feel free to contact us.

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[Analysis Case] (S)TEM Observation by Negative Staining

Examples of morphological observation of liposomes, CNF, microparticles, proteins, etc.!

Our organization offers (S)TEM observation using negative staining. Organic functional materials, such as fine particles and fibrous substances, are primarily composed of light elements like C (carbon), H (hydrogen), O (oxygen), and N (nitrogen), which do not provide sufficient contrast for morphological observation in (S)TEM. Therefore, by applying staining to these materials, we can enhance the contrast and enable observation. In this instance, we will introduce a case where negative staining was performed using phosphotungstic acid (H3[P(W3O10)4]·nH2O, abbreviated as PTA). 【Measurement Method / Processing Method】 ■ [(S)TEM] Scanning Transmission Electron Microscopy ■ Others *For more details, please download the PDF or feel free to contact us.

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[Analysis Case] (S)TEM Observation of Polymer Materials Using Electronic Staining

We will introduce examples of observing polymer materials using SEM-STEM and (S)TEM!

Our organization offers (S)TEM observation of polymer materials using electron staining. Since polymer materials are composed of light elements, it is difficult to obtain clear contrast in (S)TEM observations. Staining can enhance the contrast for such materials. This document introduces examples of staining and observation using a method called electron staining with ruthenium tetroxide (RuO4), osmium tetroxide (OsO4), and phosphotungstic acid (H3[P(W3O10)4]·xH2O, abbreviated as PTA). [Measurement and Processing Methods] ■ [(S)TEM] (Scanning) Transmission Electron Microscopy ■ Others *For more details, please download the PDF or feel free to contact us.

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[Analysis Case] Precursor Adsorption Simulation in ALD Film Formation

Information on the activation energy and reaction heat during precursor adsorption on the substrate can be obtained!

Our organization is conducting simulations of precursor adsorption in ALD film deposition using first-principles calculations. ALD (Atomic Layer Deposition) is a film deposition technology that utilizes continuous chemical reactions in the gas phase. It is widely used in the semiconductor field, where fine processing is required, due to its ability to precisely control film thickness, operate at low temperatures, and provide good step coverage. In general, to understand the differences in film deposition rates between different substrates in the slow deposition process of ALD, it is necessary to elucidate the precursor adsorption mechanisms on the substrate. [Measurement Methods and Processing Techniques] ■ Computational Science, AI, Data Analysis *For more details, please download the PDF or feel free to contact us.

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[Analysis Case] Evaluation of Crystallinity of Carbon Materials Using Raman Mapping

It is possible to visualize the in-plane distribution of materials and crystallinity non-destructively!

Our organization offers evaluation of the crystallinity of carbon materials using Raman mapping. Carbon materials possess different properties depending on their structure and crystallinity, and are used in various applications such as industrial components and medical devices. Linking the characteristics of materials to their crystallinity is effective as an indicator for material development. This document presents a case study where the in-plane distribution (peak intensity) of diamond particles, a carbon material applied to the surface of components, and the crystallinity (full width at half maximum) of each diamond particle were evaluated using Raman mapping. Diamonds exhibit a sharp peak observed sensitively at 1330 cm-1, making Raman evaluation effective. [Measurement Method / Processing Method] ■ [Raman] Raman Spectroscopy *For more details, please download the PDF or feel free to contact us.

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[Analysis Case] Evaluation of Composition Distribution of Organic Films by Raman Mapping

It is possible to visualize the in-plane distribution of organic components (inorganic components can also be included)!

Our organization offers composition distribution evaluation of organic films using Raman mapping. The properties such as mechanical characteristics, thermal resistance, and durability change by mixing materials. It is important to link material properties with mixing conditions in material development, and using dispersion as an indicator is effective. This document presents a case study of mapping the distribution of PS (polystyrene) and PCL (polycaprolactone) using Raman. By comparing the characteristic Raman peaks of each material, it is possible to separate the components of the mixture. Component separation from PCL was performed through spectral analysis around the PS-specific peak at approximately 3050 cm-1. [Measurement Method / Processing Method] ■ [Raman] Raman Spectroscopy *For more details, please download the PDF or feel free to contact us.

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[Analysis Case] Imaging of the Cuticle

It is possible to evaluate the distribution of components in the hair cuticle!

Our organization offers imaging of cuticles. The evaluation of cuticles has been limited to structural observation using electron microscopy due to their fine structure, and detailed component distribution has remained unclear. By using TOF-SIMS, which can evaluate the distribution of inorganic and organic materials at the sub-micron level, it is possible to assess the distribution of various components within the cuticle. This document presents the results of evaluating hair and visualizing the component distribution within the cuticle. [Measurement and Processing Method] ■ [TOF-SIMS] Time-of-Flight Secondary Ion Mass Spectrometry *For more details, please download the PDF or feel free to contact us.

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[Analysis Case] Dynamic Viscoelastic Evaluation of PDMS using AFM

Introduction to the evaluation of in-plane distribution of viscoelasticity and frequency dependence!

Our organization offers dynamic viscoelastic evaluation of PDMS using AFM. Dynamic Mechanical Analysis (DMA) is an effective method for investigating viscoelastic behavior, which is an important factor in the research and development of polymer materials. Additionally, by combining it with the AFM mechanism, it becomes possible to measure in-plane distribution and evaluate localized areas. This document presents a case study using AFM-DMA to map the viscoelastic modulus of PDMS (polydimethylsiloxane) and conduct frequency-dependent spectroscopy evaluation. [Measurement Method / Processing Method] ■ [AFM] Atomic Force Microscopy *For more details, please download the PDF or feel free to contact us.

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[Analysis Case] Evaluation of DC Voltage Dependence of Carriers in Semiconductors

We will introduce an analysis case using Si samples with known carrier concentration!

Our organization offers evaluation of the direct current voltage dependence of carriers in semiconductors. SMM measurement is a technique that can map the concentration of carriers in semiconductors. Additionally, it is possible to apply a direct current voltage to the sample during SMM measurement to induce carriers while measuring. Mapping measurements are conducted while acquiring SMM signals under different applied voltage conditions at each measurement point, constructing a data cube. After collecting all data, analyzing the SMM signals according to the applied voltage conditions allows us to visualize the behavior of carriers in response to the applied voltage. [Measurement Method / Processing Method] ■ [SMM] Scanning Microwave Microscope Method *For more details, please download the PDF or feel free to contact us.

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[Analysis Case] Structural Evaluation of Lithium-Ion Secondary Battery Anode Materials

The structure of the active material and current collector of secondary batteries can be evaluated in three dimensions!

Our organization offers structural evaluation of lithium-ion secondary battery anode materials. The structural state of the anode materials, such as the dispersion of active substances and porosity, affects performance. In this case, we observed the internal structure of the anode material using X-ray CT, which allows for non-destructive and high-resolution measurement of the three-dimensional structure. By analyzing the results obtained from X-ray CT, it is also possible to detect foreign substances within the electrode material and evaluate the porosity of the active substance layer. [Measurement Method / Processing Method] ■ X-ray CT Method *For more details, please download the PDF or feel free to contact us.

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[Analysis Case] Three-Dimensional Structural Analysis of 3D Printed Objects

We will utilize the measurement and analysis of the product's three-dimensional structure for quality control!

Our organization offers three-dimensional structural analysis of 3D printed objects. Understanding the differences between the design drawings and the manufactured products is an important process in quality control. By conducting X-ray CT measurements, it becomes possible to compare the three-dimensional structural "discrepancies" between the printed objects and the design drawings, allowing for an evaluation of the quality. In this case study, we are evaluating molded products made from resin-based materials, but similar evaluations can also be conducted for molded products made from metal-based materials that allow X-rays to pass through. [Measurement Method / Processing Method] ■ X-ray CT Method *For more details, please download the PDF or feel free to contact us.

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[Analysis Case] Evaluation of Mechanical Properties of Hair Cross-Sections Prepared by Microtome Method

It is possible to evaluate the elastic modulus of the internal structure of soft materials.

When evaluating the internal structure of materials, it is necessary to expose the internal structure while maintaining it through cross-sectional processing techniques such as cutting and polishing. This document introduces a case where the microtome method, which has a relatively small impact from processing damage, was used to create cross-sections of hair, followed by AFM observation of the internal structure and evaluation of elastic modulus. The microtome method is a cutting processing technique widely used in the field of soft materials, such as rubber materials and biological samples, and this approach has made it possible to evaluate the mechanical properties of the internal structure of these materials. [Measurement and Processing Methods] [AFM] Atomic Force Microscopy [AFM-MA・AFM-DMA] Mechanical Property Evaluation (Elastic Modulus Measurement, Dynamic Viscoelasticity Measurement) Ultra Microtome Processing *For more details, please download the PDF or feel free to contact us.

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[Analysis Case] Local Area Evaluation of Positive Electrode Active Material in Secondary Batteries (C0614)

Composition, crystal structure, and chemical state evaluation near the surface of living materials are possible!

Our company conducts local area evaluation of positive electrode active materials for secondary batteries (C0614). It is known that in lithium-ion secondary batteries, the crystal structure of the active material surface and the valence of metal elements change due to ion extraction and insertion during charge and discharge, as well as degradation. In a case where TEM was used for local area evaluation to assess composition, crystal structure, and chemical state, it was found through EDX that AlOx is coated on the outermost layer. Additionally, electron diffraction and EELS revealed that the crystal structure and valence differ between the surface and the interior of the active material. [Measurement and Processing Methods] ■ [(S)TEM] Scanning Transmission Electron Microscopy ■ [TEM-EDX] Energy Dispersive X-ray Spectroscopy (TEM) ■ [TEM-EELS] Electron Energy Loss Spectroscopy *For more details, please download the PDF or feel free to contact us.

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[Analysis Case] Particle Size Analysis of Au Nanoparticles Using X-ray Small Angle Scattering Method

SAXS analysis allows for the understanding of the statistical distribution of particle sizes! It can be evaluated in situ regardless of whether in a solid or liquid state.

We offer particle size analysis of Au nanoparticles using small-angle X-ray scattering (SAXS) method. Metal nanoparticles are known to exhibit unique properties not found in bulk metals. Due to their high catalytic activity and optical properties such as surface plasmon resonance, they are used in applications like fuel cell electrode catalysts and biosensors. To control these properties, it is necessary to understand their structure and composition. By using TEM and SAXS complementarily, it is possible to conduct reliable particle size analysis. [Measurement and Processing Methods] ■ [(S)TEM] Scanning Transmission Electron Microscopy ■ [SAXS] Small-Angle X-ray Scattering *For more details, please download the PDF or feel free to contact us.

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[Analysis Case] Evaluation of Stainless Steel Passive Films Compliant with SEMI Standards

Evaluation indicators regarding passive film properties can be obtained through standardized testing!

We offer the evaluation of stainless steel passive films in accordance with SEMI standards (C0612). Stainless steel exhibits excellent corrosion resistance due to the formation of a very thin, dense, and stable chromium oxide film (passive film) on its surface. The composition and film thickness of this passive film can be effectively evaluated using surface-sensitive techniques such as XPS and AES. [Measurement and Processing Methods] ■ [AES] Auger Electron Spectroscopy ■ [XPS] X-ray Photoelectron Spectroscopy ■ Others *For more details, please download the PDF or feel free to contact us.

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[Analysis Case] Identification Analysis of Pigments by Direct MS Method (C0611)

Estimate the molecular weight, chemical formula, and structural formula of pigments using a high-resolution mass spectrometer!

We offer identification analysis of pigments using the direct MS method (C0611). Due to the insolubility of pigments in solvents, chromatographic separation is not possible, and the analytical methods are limited. However, evaluation can be performed using the direct MS method, which directly introduces the sample into the mass spectrometer. There are several techniques within the direct MS method, and it is necessary to choose the appropriate one based on the properties of the sample. In a case where pigments in toner were measured, molecular ions were detected, allowing for structural estimation. [Measurement and Processing Methods] ■ Others *For more details, please download the PDF or feel free to contact us.

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[Analysis Case] SEM Observation of Wide-Area Cross-Section Using Xe-PFIB

Observation of cross-sections with an accuracy of several tens of nanometers and a size of several hundred micrometers is possible!

We offer wide-area cross-sectional SEM observation (C0610) using Xe-PFIB. The metal bonding that electrically connects the electrodes of integrated circuits, electrodes, printed circuit boards, and semiconductor packages has a diameter of several tens of μm to several hundred μm. With Xe-PFIB (Xe-Plasma Focused Ion Beam), we can target processing positions on the order of several tens of nm and create cross-sections of several hundred μm square, allowing for a detailed understanding of the entire view at the center of the bonding. 【Measurement and Processing Methods】 ■ [SEM] Scanning Electron Microscopy ■ X-ray CT Method ■ [FIB] Focused Ion Beam Processing *For more details, please download the PDF or feel free to contact us.

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[Analysis Case] Theoretical Calculation of Fe/MgO/Fe Junction System (C0583)

Investigation of TMR ratio and the behavior of spin and charge in the Fe/MgO/Fe junction system using first-principles calculations with the NEGF method!

Our company is conducting theoretical calculations (C0583) on the Fe/MgO/Fe junction system that demonstrates the tunnel magnetoresistance effect of MRAM. Tunnel magnetoresistance (TMR) is a phenomenon where the electrical resistance changes depending on the orientation of magnetization in ferromagnetic layers separated by a thin insulating layer, and applications in magnetic resistance memory (MRAM) are being advanced. Through simulations, it is also possible to evaluate the effects of behaviors under bias application, strain at the interface, and oxygen vacancies on the physical properties of TMR. 【Measurement Methods and Processing Methods】 ■ Computational Science, AI, Data Analysis *For more details, please download the PDF or feel free to contact us.

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[Analysis Case] Composite Analysis of Specific Areas within Electronic Devices (C0572)

Non-destructive assessment of specific areas inside the device! Evaluation of detailed structure and composition information of specific areas through cross-sectional observation.

Our company offers technologies suitable for structural evaluation of electronic devices, and we propose analytical methods tailored to the observation field and objectives. In a case where we investigated specific areas of a device using X-ray CT and FIB-SEM, we first used X-ray CT to observe the internal structure of the entire sample and identify specific areas. Next, we used FIB-SEM to confirm the detailed structure of the specific structures identified on the vias. 【Measurement and Processing Methods】 ■[SEM] Scanning Electron Microscopy ■[SEM-EDX] Energy Dispersive X-ray Spectroscopy (SEM) ■X-ray CT Method ■[FIB] Focused Ion Beam Processing *For more details, please download the PDF or feel free to contact us.

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  • 【イプロス初主催】AIを活用したリアル展示会!出展社募集中

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